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Admissions
It is a University which is committed to excellence and overall development of the student...
Placements
Excellent education not only imparts knowledge, but also paves the way for...
Life@IIS Univ
Life @ IISU is nothing less than a kaleidoscope of myriad hues; complete with...
Academics
Taking the age-old tradition of enlightenment through education forward,...
Research
To stimulate curiosity and cater to the global needs of a dynamic education,...
About Us
The IIS University, with its perfect amalgamation of innovation, inspiration...

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Chemistry - Semester III https://chemistry.iisuniv.ac.in/semester/semester-iii en Mathematical & Scientific Aptitude Course https://chemistry.iisuniv.ac.in/courses/subjects/mathematical-scientific-aptitude-course-0 <div class="field field-name-field-paper-code field-type-text field-label-inline clearfix"><div class="field-label">Paper Code: </div><div class="field-items"><div class="field-item even">25GSAS320</div></div></div><div class="field field-name-field-credits field-type-text field-label-inline clearfix"><div class="field-label">Credits: </div><div class="field-items"><div class="field-item even">4</div></div></div><div class="field field-name-field-periods field-type-number-decimal field-label-inline clearfix"><div class="field-label">Contact Hours: </div><div class="field-items"><div class="field-item even">60.00</div></div></div><div class="field field-name-field-maxmarks field-type-number-decimal field-label-inline clearfix"><div class="field-label">Max. Marks: </div><div class="field-items"><div class="field-item even">100.00</div></div></div><div class="field field-name-field-objective field-type-text-long field-label-above"><div class="field-label">Objective: </div><div class="field-items"><div class="field-item even"><p><strong>This course will enable the students to </strong></p> <h5>develop a conceptual understanding of higher mathematical aptitude, non-verbal ability, data interpretation and general science concepts & applications.</h5> <p> </p> </div></div></div><div class="field field-name-field-course-outcomes field-type-text-with-summary field-label-above"><div class="field-label">Course Outcomes: </div><div class="field-items"><div class="field-item even"><table border="1" cellpadding="0" cellspacing="0" id="tab" style="width: 100%" width="743"> <thead> <tr> <th colspan="2" scope="col" style="width: 155px; height: 36px;"> <p align="center"><strong>Course</strong></p> </th> <th rowspan="2" scope="col" style="width: 211px; height: 36px;"> <p> </p> <p><strong>Course Outcomes</strong></p> </th> <th rowspan="2" scope="col" style="width: 120px; height: 36px;"> <p><strong>Learning and Teaching Strategies</strong></p> </th> <th rowspan="2" scope="col" style="width: 108px; height: 36px;"> <p><strong>Assessment                Strategies</strong></p> </th> </tr> </thead> <tbody> <tr> <td style="width:66px;height:36px;"> <p><strong>Course code</strong></p> </td> <td style="width:89px;height:36px;"> <p><strong>Course Title</strong></p> </td> </tr> <tr> <td style="width:66px;height:89px;"> <p><strong>24GSAS 320</strong></p> </td> <td style="width:89px;height:89px;"> <p align="center">Mathematical & Scientific Aptitude Course</p> <p align="center">(TheorC07 y)</p> <p> </p> </td> <td style="width:211px;height:89px;"> <p>CO7 Prioritize and develop mathematical skills and attitude to meet  the demands of (i) daily life (ii) future mathematical work and (iii) work in the related fields of knowledge.</p> <p>CO8 To improve and combine the communication between people and create a strategy that specializes in understanding others' communication and using that knowledge to interact productively.</p> <p>CO9 Develop and estimate appropriate approximations. To distinguish the concept of ratio and scale drawing, examine graphs, diagrams and tables.</p> <p>CO10 Discover and develop aesthetic sensibilities and process skills.</p> <p>C011 To develop inquiring minds and curiosity about science and nature. to analyze knowledge, conceptual understanding, and skills to solve problems.</p> <p>C012 Contribute effectively in course-specific interaction.</p> </td> <td style="width:120px;height:89px;"> <p><strong>Approach in</strong></p> <p><strong>teaching:                 </strong>Interactive</p> <p>Lectures,               Discussion, assignments; Solving Questions.</p> <p> </p> <p><strong>Learning activities for the students: </strong>Self- learning assignments, Effective questions.</p> </td> <td style="width:108px;height:89px;"> <p>Class test, Unit end examinations, Quiz, Solving problems in Assignments.</p> </td> </tr> </tbody> </table> <p> </p> </div></div></div><div class="field field-name-field-unit1hours field-type-number-decimal field-label-hidden"><div class="field-items"><div class="field-item even">12.00</div></div></div><div class="field field-name-field-unit1title field-type-text field-label-above"><div class="field-label">Unit I: </div><div class="field-items"><div class="field-item even"> HIGHER MATHEMATICAL APTITUDE </div></div></div><div class="field field-name-field-unit1description field-type-text-long field-label-hidden"><div class="field-items"><div class="field-item even"><ul> <li align="left">Sequence & Series</li> <li align="left">Permutation & Combination</li> <li align="left">Probability</li> <li align="left">Mensuration</li> <li align="left">Geometry</li> <li align="left">Coordinate Geometry</li> <li align="left">Trigonometry</li> <li align="left">Algebra</li> </ul> <p> </p> </div></div></div><div class="field field-name-field-unit2hours field-type-number-decimal field-label-hidden"><div class="field-items"><div class="field-item even">12.00</div></div></div><div class="field field-name-field-unit2title field-type-text field-label-above"><div class="field-label">Unit II: </div><div class="field-items"><div class="field-item even">NON-VERBAL ABILITY </div></div></div><div class="field field-name-field-unit2description field-type-text-long field-label-hidden"><div class="field-items"><div class="field-item even"><ul> <li align="left">Mirror Images</li> <li align="left">Water Images</li> <li align="left">Paper Folding & Cutting</li> <li align="left">Non-Verbal Analogy</li> <li align="left">Non-Verbal Classification</li> <li align="left">Non-Verbal Series</li> <li align="left">Embedded Figure</li> <li align="left">Completion of Figure</li> </ul> <p> </p> </div></div></div><div class="field field-name-field-unit3hours field-type-number-decimal field-label-hidden"><div class="field-items"><div class="field-item even">12.00</div></div></div><div class="field field-name-field-unit3title field-type-text field-label-above"><div class="field-label">Unit III: </div><div class="field-items"><div class="field-item even">DATA INTERPRETATION & GRAPHICAL ANALYSIS </div></div></div><div class="field field-name-field-unit3description field-type-text-long field-label-hidden"><div class="field-items"><div class="field-item even"><ul> <li align="left">Data-Meaning & Types</li> <li align="left">Measures of Central Tendency</li> <li align="left">Graphical Analysis : Bar Graph, Line Graph</li> <li align="left">Pie Chart</li> <li align="left">Tabulation of Data</li> </ul> <p> </p> </div></div></div><div class="field field-name-field-unit4hours field-type-number-decimal field-label-hidden"><div class="field-items"><div class="field-item even">12.00</div></div></div><div class="field field-name-field-unit4title field-type-text field-label-above"><div class="field-label">Unit IV: </div><div class="field-items"><div class="field-item even">GENERAL SCIENCE- CONCEPTS </div></div></div><div class="field field-name-field-unit4description field-type-text-long field-label-hidden"><div class="field-items"><div class="field-item even"><ul> <li align="left">Physical Concepts</li> <li align="left">Chemical Concepts</li> <li align="left">Biological Concepts & Human Body</li> </ul> <p> </p> </div></div></div><div class="field field-name-field-unit5hours field-type-number-decimal field-label-hidden"><div class="field-items"><div class="field-item even">12.00</div></div></div><div class="field field-name-field-unit5title field-type-text field-label-above"><div class="field-label">Unit V: </div><div class="field-items"><div class="field-item even">GENERAL SCIENCE- APPLICATIONS </div></div></div><div class="field field-name-field-unit5description field-type-text-long field-label-hidden"><div class="field-items"><div class="field-item even"><ul> <li align="left">General Diseases & Deficiencies</li> <li align="left">Nutrients</li> <li align="left">Instruments & Innovations</li> </ul> <p> </p> </div></div></div><div class="field field-name-field-essential-reading field-type-text-long field-label-above"><div class="field-label">Essential Readings: </div><div class="field-items"><div class="field-item even"><ol> <li align="left">Algebra & Trigonometry by Jay Abramson</li> <li align="left">Basic Mathematics by Serge Lang</li> <li align="left">Non-Verbal Reasoning by R.S. Agarwal</li> <li align="left">NCERT Science</li> </ol> <p> </p> </div></div></div><div class="field field-name-field-references field-type-text-long field-label-above"><div class="field-label">References: </div><div class="field-items"><div class="field-item even"><ol> <li align="left">NCERT Exemplar Mathematics</li> <li align="left">Physics by S.C. Verma</li> <li align="left">Encyclopedia Britannica</li> <li align="left">The Elements of Chemistry by Antoine Lavoisier.</li> </ol> <p> </p> <h5><strong>a.</strong><strong>Resources:</strong></h5> <ol> <li align="left"><a href="https://epathshala.nic.in/">https://epathshala.nic.in/</a></li> <li align="left"><a href="https://egyankosh.ac.in/">https://egyankosh.ac.in/</a></li> </ol> <p> </p> <p align="left"> </p> <p> </p> </div></div></div><div class="field field-name-field-academic-year field-type-taxonomy-term-reference field-label-above"><div class="field-label">Academic Year: </div><div class="field-items"><div class="field-item even"><a href="/academic-year/2025-2026" typeof="skos:Concept" property="rdfs:label skos:prefLabel" datatype="">2025-2026</a></div></div></div> Mon, 02 Jun 2025 09:27:07 +0000 ruchi.singh@iisuniv.ac.in 1980 at https://chemistry.iisuniv.ac.in Physical Chemistry Lab II https://chemistry.iisuniv.ac.in/courses/subjects/physical-chemistry-lab-ii-10 <div class="field field-name-field-paper-code field-type-text field-label-inline clearfix"><div class="field-label">Paper Code: </div><div class="field-items"><div class="field-item even">25CHY328</div></div></div><div class="field field-name-field-credits field-type-text field-label-inline clearfix"><div class="field-label">Credits: </div><div class="field-items"><div class="field-item even">3</div></div></div><div class="field field-name-field-periods field-type-number-decimal field-label-inline clearfix"><div class="field-label">Contact Hours: </div><div class="field-items"><div class="field-item even">90.00</div></div></div><div class="field field-name-field-maxmarks field-type-number-decimal field-label-inline clearfix"><div class="field-label">Max. Marks: </div><div class="field-items"><div class="field-item even">100.00</div></div></div><div class="field field-name-field-objective field-type-text-long field-label-above"><div class="field-label">Objective: </div><div class="field-items"><div class="field-item even"><p><strong>This course will enable the students to </strong></p> <p>develop advanced hands on experience in the operation of conductivity meter, dropping mercury electrode and potentiometer and acquire the knowledge of basic terminology regarding conductance, chemical kinetics, adsorption, polarography and potentiometry.</p> <p> </p> </div></div></div><div class="field field-name-field-course-outcomes field-type-text-with-summary field-label-above"><div class="field-label">Course Outcomes: </div><div class="field-items"><div class="field-item even"><table border="1" cellpadding="0" cellspacing="0" id="tab" style="width: 100%" width="106%"> <thead> <tr> <th colspan="2" scope="col" style="width: 26.12%; height: 23px;"> <p><strong>Course</strong></p> </th> <th rowspan="2" scope="col" style="width: 32.98%; height: 23px;"> <p><strong>Learning outcome</strong></p> <p><strong>(at course level)</strong></p> </th> <th rowspan="2" scope="col" style="width: 22.04%; height: 23px;"> <p><strong>Learning and Teaching Strategies</strong></p> </th> <th rowspan="2" scope="col" style="width: 18.88%; height: 23px;"> <p><strong>Assessment Strategies </strong></p> </th> </tr> </thead> <tbody> <tr> <td style="width:11.54%;height:23px;"> <p align="center"><strong>Course Code</strong></p> </td> <td style="width:14.56%;height:23px;"> <p align="center"><strong>Course</strong></p> <p align="center"><strong>Title</strong></p> </td> </tr> <tr> <td style="width:11.54%;"> <p> </p> <p align="center"><strong>25CHY328</strong></p> </td> <td style="width:14.56%;"> <p align="center"> </p> <p>Physical Chemistry Lab II</p> <p align="center"><strong> (Practical)</strong></p> </td> <td style="width:32.98%;"> <p>CO133 Calibrate and operate a variety of scientific instruments to perform experiments based on chemical kinetics, potentiometry, polarography, electrochemistry, and adsorption and explain the principle behind the experiments.</p> <p>CO134 Perform scientific experiments as well as accurately record experimental data and analyze the results of such experiments.</p> <p>CO135 Contribute effectively in course-specific interaction.</p> </td> <td style="width:22.04%;"> <p><strong>Approach in teaching:</strong></p> <p>Laboratory instructions and</p> <p>Demonstrations.</p> <p> </p> <p><strong>Learning activities for the students:</strong></p> <p>Peer learning, hands-on-learning,</p> <p>interpretation of data, record writing and learning through virtual labs</p> <p> </p> </td> <td style="width:18.88%;"> <p>Conduction of Experiments, Lab Records, Viva Voce, Quiz</p> </td> </tr> </tbody> </table> <p> </p> </div></div></div><div class="field field-name-field-unit1title field-type-text field-label-above"><div class="field-label">Unit I: </div><div class="field-items"><div class="field-item even"> </div></div></div><div class="field field-name-field-unit1description field-type-text-long field-label-hidden"><div class="field-items"><div class="field-item even"><p>A list of experiments under different headings is given below. Students are required to perform at least 8-10 experiments.</p> <p> </p> <p><strong>Chemical Kinetics</strong></p> <ol style="list-style-type:lower-roman;"> <li>To determine the effect of (a) change of temperature (b) change of concentration of reactants and (c) catalysts on the velocity constant of hydrolysis of an ester.</li> <li>To study the kinetics of the reaction between K<sub>2</sub>S<sub>2</sub>O<sub>8</sub> (potassium persulphate) and KI (potassium iodide) and to determine the rate constant and the energy of activation of the reaction.</li> <li>To determine of primary salt effect in the kinetics of ionic reaction and to test the Bronsted relationship (Iodide ion is oxidized by persulphate ion).</li> <li>To study the kinetics of saponification of ethyl acetate by sodium hydroxide and to determine the rate constant.</li> <li>To determine the rate constant, energy of activation and entropy of activation in the oxidation of benzyl alcohol (C<sub>6</sub>H<sub>5</sub>CH<sub>2</sub>OH) by potassium permanganate in acidic medium.</li> <li>To determine the formation constant for the (Ce<sup>+4</sup>-H<sub>3</sub>PO<sub>2</sub>) intermediate complex and its decomposition rate constant at the room temperature.</li> <li>To determine the rate constant for the bleaching of malachite green in basic medium at room temperature spectrophotometrically.</li> <li>To determine the rate constant, order of reaction and energy of activation for saponification of ethyl acetate using NaOH conductometrically.</li> </ol> <p> </p> <p><strong>Electrochemistry </strong></p> <ol style="list-style-type:lower-roman;"> <li>To estimate the concentration of H<sub>2</sub>SO<sub>4</sub>, CH<sub>3</sub>COOH and CuSO<sub>4</sub> by conductometric titration using NaOH solution.</li> <li>To determine equivalent conductance of the strong electrolytes (KCl, HNO<sub>3</sub>, HCl etc.) at several concentrations and to verify the Onsagar’s equation and find the values of a and b in the equation.</li> <li>To determine the equivalent conductance of acetic acid at infinite dilution and to calculate its degree of dissociation at different dilutions as well as dissociation constant at the room temperature.</li> </ol> <p> </p> <p><strong>Potentiometry </strong></p> <ol style="list-style-type:lower-roman;"> <li>To determine the concentration of ferrous ion in the given solution by titrating against N/10 Cr<sub>2</sub>O<sub>7</sub><sup>--</sup> or Ce<sup>+4</sup> ion solution and also determine the equivalence point by plotting E <em>vs.</em> V, ∆E <em>vs. </em>∆V and ∆<sup>2</sup>E/∆V<sup>2 </sup><em>vs. </em>∆V.</li> </ol> <p> </p> <p><strong>Polarography (demonstration)</strong></p> <ol style="list-style-type:lower-roman;"> <li>To determine the half wave potentials of Cd<sup>+2</sup> and Zn<sup>+2</sup> ions in 0.1 M KCl solution and to show that half wave potential is independent of the concentration.</li> </ol> <p> </p> <p><strong>Adsorption </strong></p> <ol style="list-style-type:lower-roman;"> <li>To study the adsorption of acetic acid or oxalic acid from aqueous solution by activated charcoal or animal charcoal and to examine the validity of Freundlich and Langmuir adsorption isotherms.</li> <li>To compare cleansing power of samples of two detergents.</li> <li>To study the variation of surface tension of solution of n-propyl alcohol with concentration and to determine the limiting cross section area of alcohol molecule.</li> <li>To determine the radius of molecule by viscosity measurements (e.g. Glycerol)</li> </ol> <p> </p> <p> </p> </div></div></div><div class="field field-name-field-unit2description field-type-text-long field-label-hidden"><div class="field-items"><div class="field-item even"><p align="center"><strong>Scheme of Examination</strong></p> <p align="center"> </p> <p>The duration of the examination will be 6 hrs.</p> <p>The following exercises will be set in the examination</p> <p>Physical Chemistry Experiment                           55 marks</p> <p>Viva                                                                  15 marks</p> <p><strong>      Total                                                                      70 marks</strong></p> <p> </p> <p> </p> <ol> <li><strong>Physical Chemistry Experiment </strong></li> </ol> <p>The exercise carries 55 marks. The candidates shall be given one exercise out of exercises prescribed in the syllabus. The exercises in physical chemistry can be modified by the examiner and the same will be explained to the candidates. However, such modifications will not involve any departure from the basic principles over which experiments are prescribed in the syllabus.</p> <p>Candidates shall be given one exercise out of the exercises prescribed in the syllabus.</p> <p>The distribution of marks will be as follows</p> <ol style="list-style-type:lower-roman;"> <li>Theory and procedure                                       10 marks</li> <li>Correct observation                                           15 marks</li> <li>Use of correct formula                                       8   marks</li> <li>Calculation                                                       15 marks</li> <li>Results                                                             7   marks</li> </ol> <p> </p> <p>No marks for calculation will be awarded to a candidate for not calculating the result.</p> <p>The permissible error will depend on the nature of the experiment. Generally, <u>+</u> 10% error may be taken as permissible error for experiments involving potentiometric and conductometric measurements. The constancy in values of rate constants may be taken into consideration while awarding marks in experiments on chemical kinetics. One mark shall be deducted for each <u>+</u> 2% error over permissible limit.</p> <p> </p> <ol> <li value="2"><strong>Viva</strong></li> </ol> <p>Oral questions shall generally be asked about the work assigned to the candidate. The purpose is to find out to what extent the candidate understood the basic principles of chemistry.</p> <p> </p> <p> </p> <p> </p> <ul> <li align="left"> </li> </ul> <p> </p> </div></div></div><div class="field field-name-field-essential-reading field-type-text-long field-label-above"><div class="field-label">Essential Readings: </div><div class="field-items"><div class="field-item even"><ol> <li>Practical Physical Chemistry; Thirtieth Edition; J. B. Yadav; Krishna Prakashan Media Pvt. Ltd., Meerut Advanced, 2011.</li> </ol> <p> </p> </div></div></div><div class="field field-name-field-references field-type-text-long field-label-above"><div class="field-label">References: </div><div class="field-items"><div class="field-item even"><p>.  Experimental Physical Chemistry, First Edition; V. D. Athawale, P. Mathur; New age International     (P) Ltd. Publishers, New Delhi, 2011.</p> <ol> <li>Experimental Physical Chemistry; R. C. Das and B. Behera; Tata Mc-Graw Hill publishing Co. Pvt. Ltd., 1993.</li> <li>Experiments in Physical Chemistry, Fifth Edition, D. P. Shoemaker, C. W. Garland and J. W. Nibler,  Mc Graw-Hill, New York, 1998.</li> <li>Introductory Practical Physical Chemistry; D. T. Burns  and E. Rattenbury, Pergamon Press, 1966.</li> </ol> <p style="margin-left:.25in;"> </p> <p style="margin-left:.25in;"><strong>e-Resources:</strong></p> <ol> <li><a href="https://vlab.amrita.edu/index.php?sub=2&brch=294&sim=687&cnt=1">https://vlab.amrita.edu/index.php?sub=2&brch=294&sim=687&cnt=1</a></li> <li><a href="https://vlab.amrita.edu/?brch=190&cnt=1&sim=606&sub=2">https://vlab.amrita.edu/?brch=190&cnt=1&sim=606&sub=2</a></li> <li><a href="https://vlab.amrita.edu/?sub=2&brch=190">https://vlab.amrita.edu/?sub=2&brch=190</a></li> <li><a href="http://web.mst.edu/~gbert/conductivity/cond.html">http://web.mst.edu/~gbert/conductivity/cond.html</a></li> <li><a href="http://vlab.amrita.edu/?sub=3&brch=190&sim=606&cnt=1">http://vlab.amrita.edu/?sub=3&brch=190&sim=606&cnt=1</a></li> </ol> <p> </p> </div></div></div><div class="field field-name-field-academic-year field-type-taxonomy-term-reference field-label-above"><div class="field-label">Academic Year: </div><div class="field-items"><div class="field-item even"><a href="/academic-year/2025-2026" typeof="skos:Concept" property="rdfs:label skos:prefLabel" datatype="">2025-2026</a></div></div></div> Mon, 02 Jun 2025 09:20:55 +0000 ruchi.singh@iisuniv.ac.in 1979 at https://chemistry.iisuniv.ac.in Organic Chemistry Lab II https://chemistry.iisuniv.ac.in/courses/subjects/organic-chemistry-lab-ii-6 <div class="field field-name-field-paper-code field-type-text field-label-inline clearfix"><div class="field-label">Paper Code: </div><div class="field-items"><div class="field-item even">25CHY327</div></div></div><div class="field field-name-field-credits field-type-text field-label-inline clearfix"><div class="field-label">Credits: </div><div class="field-items"><div class="field-item even">3</div></div></div><div class="field field-name-field-periods field-type-number-decimal field-label-inline clearfix"><div class="field-label">Contact Hours: </div><div class="field-items"><div class="field-item even">90.00</div></div></div><div class="field field-name-field-maxmarks field-type-number-decimal field-label-inline clearfix"><div class="field-label">Max. Marks: </div><div class="field-items"><div class="field-item even">100.00</div></div></div><div class="field field-name-field-objective field-type-text-long field-label-above"><div class="field-label">Objective: </div><div class="field-items"><div class="field-item even"><p><strong>This course will enable the students to </strong></p> <p>acquire knowledge of synthesis by conventional and non-conventional methods, handling of hazardous chemicals and to enhance learning of physical and spectroscopic techniques.</p> <p> </p> </div></div></div><div class="field field-name-field-course-outcomes field-type-text-with-summary field-label-above"><div class="field-label">Course Outcomes: </div><div class="field-items"><div class="field-item even"><table border="1" cellpadding="0" cellspacing="0" id="tab" style="width: 100%" width="103%"> <thead> <tr> <th colspan="2" scope="col" style="width: 27.04%; height: 23px;"> <p><strong>Course</strong></p> </th> <th rowspan="2" scope="col" style="width: 31.4%; height: 23px;"> <p><strong>Learning outcome</strong></p> <p><strong>(at course level)</strong></p> </th> <th rowspan="2" scope="col" style="width: 22.86%; height: 23px;"> <p><strong>Learning and Teaching Strategies</strong></p> </th> <th rowspan="2" scope="col" style="width: 18.7%; height: 23px;"> <p><strong>Assessment Strategies </strong></p> </th> </tr> </thead> <tbody> <tr> <td style="width:11.86%;height:23px;"> <p align="center"><strong>Course Code</strong></p> </td> <td style="width:15.18%;height:23px;"> <p align="center"><strong>Course</strong></p> <p align="center"><strong>Title</strong></p> </td> </tr> <tr> <td style="width:11.86%;"> <p> </p> <p align="center"><strong>25CHY327</strong></p> </td> <td style="width:15.18%;"> <p align="center"> </p> <p align="center">Organic Chemistry Lab II</p> <p align="center"><strong>(Practical)</strong></p> </td> <td style="width:31.4%;"> <p>C0129 Characterize organic molecules by different spectral techniques.</p> <p>CO130 Demonstrate and apply common laboratory techniques for organic synthesis.</p> <p>CO131 Employ spectrophotometric techniques for the estimations of prescribed biomolecules.</p> <p>CO132 Contribute effectively in course-specific interaction.</p> </td> <td style="width:22.86%;"> <p><strong>Approach in teaching:</strong></p> <p>Laboratory instructions and</p> <p>Demonstrations.</p> <p> </p> <p><strong>Learning activities for the students:</strong></p> <p>Peer learning, hands-on-learning,</p> <p>interpretation of data, record writing and learning through virtual labs</p> <p> </p> </td> <td style="width:18.7%;"> <ul> <li align="left">Conduction of Experiments, Lab Records, Viva Voce, Quiz</li> </ul> </td> </tr> </tbody> </table> <p> </p> </div></div></div><div class="field field-name-field-unit1title field-type-text field-label-above"><div class="field-label">Unit I: </div><div class="field-items"><div class="field-item even"> </div></div></div><div class="field field-name-field-unit1description field-type-text-long field-label-hidden"><div class="field-items"><div class="field-item even"><p><strong>Green Chemistry                                                                                                    </strong></p> <p>Green Chemistry & sustainability, twelve principles of green chemistry, atom economy, E-factor, green chemistry tools.</p> <p>Solvents:Types based on hazards, applications, green solvents-supercritical fluids, ionic liquids, water, solvent free solid phase reaction.</p> <p>Alternative energy sources, ultrasound, microwave, reactions at high pressure in constrained media, renewable sources, C1 chemistry.</p> <p>Green catalysts-types, advantages and disadvantages, applications in organic synthesis.</p> <p style="margin-left:.25in;"><strong>Synthesis (Green Methods / Conventional Methods)                                             (30 Hours)</strong></p> <ol style="list-style-type:lower-alpha;"> <li align="left"><strong>One step synthesis</strong> <ul> <li align="left">Aldol condensation (Synthesis of dibenzal propanone)</li> <li align="left">Acetylation (synthesis of acetanilide from aniline)</li> <li align="left">Pechmann Condensation for Coumarin synthesis (Clay catalyzed solid state synthesis of 7- hydroxy -4-methyl coumarin)</li> <li align="left">Bromination of phenol</li> </ul> </li> </ol> <p style="margin-left:.25in;"> </p> <ol style="list-style-type:lower-alpha;"> <li align="left" value="2"><strong>Two step synthesis (any three)</strong> <ul> <li align="left">Benzoin → benzil → benzilic acid</li> <li align="left">Benzophenone → benzopinacol → benzopinacolone</li> <li align="left">Acetanilide → p-bromoacetanilide → p-bromoaniline</li> <li align="left">Acetanilide → p-nitroacetanilide → p-nitroaniline</li> <li align="left">Resorcinol → fluorescein → eosin</li> <li align="left">Phthalic anhydride → phthalimide → anthranilic acid</li> </ul> </li> </ol> <h2> </h2> <h2><span style="font-size:12px;">Extraction of Organic Compounds from Natural Resources (any three)   </span>            </h2> <ul> <li align="left">Isolation of caffeine from tea leaves.</li> <li align="left">Isolation of casein from milk.</li> <li align="left">Isolation of lactose from milk.</li> <li align="left">Isolation of nicotine dipicrate from tobacco.</li> </ul> <h2> </h2> <h2><span style="font-size:12px;">Spectroscopy                                                                                                             </span></h2> <p style="margin-left:.25in;">Identification of organic compounds (with emphasis on isomeric studies and calculation of % ratio of tautomers) by the spectral analysis.</p> <h2><span style="font-size:12px;">Spectrophotometric Estimations</span> <span style="font-size:12px;">(any three)   </span>                                                       </h2> <ul> <li align="left">Protein</li> <li align="left">Carbohydrate</li> <li align="left">Cholesterol</li> <li align="left">Phosphate</li> <li align="left">Ascorbic acid</li> </ul> <p style="margin-left:.25in;"> </p> <p> </p> </div></div></div><div class="field field-name-field-unit2description field-type-text-long field-label-hidden"><div class="field-items"><div class="field-item even"><p align="center"><strong>Scheme of Examination</strong></p> <p align="center"> </p> <p>The duration of examination will be 6 hrs.</p> <p>The following exercises will be set in the examination</p> <p>Organic Synthesis                                                         26 marks</p> <p>Spectral Problems                                                          14 marks</p> <p>Spectrophotometric Estimation                                      15 marks</p> <p>Viva                                                                             15 marks</p> <p><strong>Total                                                                               70 marks </strong></p> <p> </p> <p><strong>1.Organic ynthesis</strong></p> <p>This exercise carries 26 marks. Either 2 one step synthesis or two step synthesis will be allotted to the candidates by lot. The yield, purity, crystallization and recording of m.p. will be given due consideration while awarding marks. </p> <p> </p> <p><strong>2.Spectral Problems </strong></p> <p>This exercise carries 14 marks. The students may be provided with either spectral problems or data base problems.</p> <p> </p> <p><strong>3.Spectrophotometric Estimation</strong></p> <p>This exercise carries 15 marks. Three marks are reserved for the preparatory work, setting up of an instrument and experimental skills. The distribution of remaining 12 marks are as follows.</p> <p>Correct observation and proper recording                                   4 marks</p> <p>Standard curve                                                                         4 marks</p> <p>Result                                                                                      4marks</p> <p> </p> <p><strong>4.Viva </strong></p> <p>Oral questions shall generally be asked over the work assigned to the candidate. The purpose is to find out as to what extent the candidate has understanding the basic principles of chemistry.</p> <p> </p> <p> </p> <p> </p> </div></div></div><div class="field field-name-field-essential-reading field-type-text-long field-label-above"><div class="field-label">Essential Readings: </div><div class="field-items"><div class="field-item even"><ol> <li>Vogel’s Textbook of Practical Organic Chemistry, Fifth Edition, B.S. Furniss, A.J. Hannaford, P.W.G. Smith, A.R. Tatchell; Addison – Wesley Publishing Company, 2014.</li> <li>Practical Organic Chemistry, Fourth Edition; F.C. Mann and B.C. Saunders; Pearson Education, New Delhi, 2013.</li> </ol> <p> </p> </div></div></div><div class="field field-name-field-references field-type-text-long field-label-above"><div class="field-label">References: </div><div class="field-items"><div class="field-item even"><ol> <li>Advanced Practical Organic Chemistry, J. Leonard, B. Lygo and G. Procter; Third Edition; CRC Press, 2013.</li> <li>Green Chemistry: Introductory Text, Third Edition; M. Lancaster; Royal Society of Chemistry (London), 2016.</li> </ol> <p style="margin-left:.25in;"> </p> <p style="margin-left:.25in;"><strong>e-Resources:</strong></p> <ol> <li value="3"><a href="https://chem.libretexts.org/Bookshelves/Ancillary_Materials/Laboratory_Experiments/Wet_Lab_Experiments/Organic_Chemistry_Labs/Experiments/3%3A_Extraction_of_Caffeine_(Experiment)">https://chem.libretexts.org/Bookshelves/Ancillary_Materials/Laboratory_Experiments/Wet_Lab_Experiments/Organic_Chemistry_Labs/Experiments/3%3A_Extraction_of_Caffeine_(Experiment)</a> (Isolation of caffeine from tea leaves)</li> <li value="4"><a href="https://youtu.be/sPhJWBL17OQ">https://youtu.be/sPhJWBL17OQ</a> (Isolation of caffeine from tea leaves)</li> <li value="5"><a href="https://vlab.amrita.edu/?sub=3&brch=63&sim=158&cnt=1">https://vlab.amrita.edu/?sub=3&brch=63&sim=158&cnt=1</a> (Isolation of casein from milk-</li> <li value="6"><a href="https://studylib.net/doc/5885894/experiment-5--isolation-of-casein-and-lactose-from-milk">https://studylib.net/doc/5885894/experiment-5--isolation-of-casein-and-lactose-from-milk</a> (Isolation of lactose from milk)</li> <li value="7"><a href="https://youtu.be/DBS5g4BoSZY">https://youtu.be/DBS5g4BoSZY</a>  (Isolation of lactose from milk) <a href="https://youtu.be/16lGxX19x9M">https://youtu.be/16lGxX19x9M</a> (Isolation of nicotine dipicrate from tobacco)</li> <li value="8"><a href="http://www.ijcrt.org/papers/IJCRT2008374.pdf">http://www.ijcrt.org/papers/IJCRT2008374.pdf</a> (Isolation of nicotine dipicrate from tobacco)</li> </ol> <p> </p> <p> </p> </div></div></div><div class="field field-name-field-academic-year field-type-taxonomy-term-reference field-label-above"><div class="field-label">Academic Year: </div><div class="field-items"><div class="field-item even"><a href="/academic-year/2025-2026" typeof="skos:Concept" property="rdfs:label skos:prefLabel" datatype="">2025-2026</a></div></div></div> Mon, 02 Jun 2025 09:04:12 +0000 ruchi.singh@iisuniv.ac.in 1975 at https://chemistry.iisuniv.ac.in Research Project – Synopsis https://chemistry.iisuniv.ac.in/courses/subjects/research-project-%E2%80%93-synopsis <div class="field field-name-field-paper-code field-type-text field-label-inline clearfix"><div class="field-label">Paper Code: </div><div class="field-items"><div class="field-item even">25CHY326</div></div></div><div class="field field-name-field-credits field-type-text field-label-inline clearfix"><div class="field-label">Credits: </div><div class="field-items"><div class="field-item even">2</div></div></div><div class="field field-name-field-periods field-type-number-decimal field-label-inline clearfix"><div class="field-label">Contact Hours: </div><div class="field-items"><div class="field-item even">60.00</div></div></div><div class="field field-name-field-maxmarks field-type-number-decimal field-label-inline clearfix"><div class="field-label">Max. Marks: </div><div class="field-items"><div class="field-item even">100.00</div></div></div><div class="field field-name-field-objective field-type-text-long field-label-above"><div class="field-label">Objective: </div><div class="field-items"><div class="field-item even"><p><strong>This course will enable the students to </strong></p> <p>Carry out extensive literature survey on a topic of choice and further take up project or dissertation on the same topic in the subsequent semester.</p> <p>Gain exposure of industries through field visits.</p> <p> </p> </div></div></div><div class="field field-name-field-course-outcomes field-type-text-with-summary field-label-above"><div class="field-label">Course Outcomes: </div><div class="field-items"><div class="field-item even"><table border="1" cellpadding="0" cellspacing="0" id="tab" style="width: 100%" width="106%"> <thead> <tr> <th colspan="2" scope="col" style="width: 27.48%; height: 23px;"> <p><strong>Course</strong></p> </th> <th rowspan="2" scope="col" style="width: 33.66%; height: 23px;"> <p><strong>Learning outcome</strong></p> <p><strong>(at course level)</strong></p> </th> <th rowspan="2" scope="col" style="width: 22.3%; height: 23px;"> <p><strong>Learning and Teaching Strategies</strong></p> </th> <th rowspan="2" scope="col" style="width: 16.56%; height: 23px;"> <p><strong>Assessment Strategies </strong></p> </th> </tr> </thead> <tbody> <tr> <td style="width:11.94%;height:23px;"> <p align="center"><strong>Course Code</strong></p> </td> <td style="width:15.54%;height:23px;"> <p align="center"><strong>Course</strong></p> <p align="center"><strong>Title</strong></p> </td> </tr> <tr> <td style="width:11.94%;"> <p> </p> <p align="center"><strong>25CHY326</strong></p> </td> <td style="width:15.54%;"> <p align="center"> </p> <p align="center"><strong>Research Project– Synopsis</strong></p> <p align="center"><strong> (Practical)</strong></p> </td> <td style="width:33.66%;"> <p><strong>CO 125:</strong> Develop the competency to systematically prepare a detailed report on an industrial visit and /or formulate a well-structured research proposal, incorporating analytical insights, methodological approaches, and relevant literature review.</p> <p><strong>CO 126: </strong>Effectively communicate technical and theoretical knowledge through structured slides, visual aids, and verbal explanations.</p> <p><strong>CO 127:</strong> Apply problem-solving skills to address complex or scenario-based questions.</p> <p><strong>CO 128:</strong> Contribute effectively in course-specific interaction.</p> <p> </p> </td> <td style="width:22.3%;"> <p><strong>Approach in teaching:</strong></p> <p>Demonstration, digital learning, field visit</p> <p> </p> <p><strong>Learning activities for the students:</strong></p> <p>Literature survey, software and instrument handling, synopsis writing</p> <p> </p> </td> <td style="width:16.56%;"> <p>Power point presentation by individual student, report writing, viva-voce.</p> </td> </tr> </tbody> </table> <p> </p> </div></div></div><div class="field field-name-field-unit1title field-type-text field-label-above"><div class="field-label">Unit I: </div><div class="field-items"><div class="field-item even"> </div></div></div><div class="field field-name-field-unit1description field-type-text-long field-label-hidden"><div class="field-items"><div class="field-item even"><p><strong>Scheme of Examination</strong></p> <p align="center"> </p> <p align="center"><strong>Continuous Assessment (30%)</strong></p> <table border="1" cellpadding="0" cellspacing="0" style="width:612px;" width="765"> <tbody> <tr> <td colspan="5" style="width:612px;height:17px;"> <p align="center"><strong>CA (Test)</strong></p> </td> </tr> <tr> <td style="width:114px;height:74px;"> <p><strong>Progress in Synopsis Preparation</strong></p> </td> <td style="width:150px;height:74px;"> <p align="center"><strong>Presentation</strong></p> </td> <td style="width:138px;height:74px;"> <p align="center"><strong>Viva </strong></p> </td> <td style="width:102px;height:74px;"> <p align="center"><strong>Attendance (Student Supervisor Interaction)</strong></p> </td> <td style="width:108px;height:74px;"> <p align="center"><strong>Total</strong></p> </td> </tr> <tr> <td style="width:114px;"> <p align="center">10</p> </td> <td style="width:150px;"> <p align="center">10</p> </td> <td style="width:138px;"> <p align="center">05</p> </td> <td style="width:102px;"> <p align="center">05</p> </td> <td style="width:108px;"> <p align="center">30</p> </td> </tr> </tbody> </table> <p align="center"> </p> <p align="center"> </p> <p align="center"><strong>Semester End Examination (70%)</strong></p> <table border="1" cellpadding="0" cellspacing="0" style="width:570px;" width="712"> <tbody> <tr> <td style="width:241px;height:49px;"> <p align="center"><strong>Report</strong></p> </td> <td style="width:136px;height:49px;"> <p align="center"><strong>Presentation</strong></p> </td> <td style="width:192px;height:49px;"> <p align="center"><strong>Viva</strong></p> </td> </tr> <tr> <td style="width:241px;"> <p align="center">40</p> </td> <td style="width:136px;"> <p align="center">15</p> </td> <td style="width:192px;"> <p align="center">15</p> </td> </tr> </tbody> </table> <p> </p> <p>To give the exposure of industries, field visits will be organized.  Students will either prepare a report of the visit or a quiz may be organized which will be evaluated in presence of panel of experts.</p> <p> </p> <p> </p> </div></div></div><div class="field field-name-field-academic-year field-type-taxonomy-term-reference field-label-above"><div class="field-label">Academic Year: </div><div class="field-items"><div class="field-item even"><a href="/academic-year/2025-2026" typeof="skos:Concept" property="rdfs:label skos:prefLabel" datatype="">2025-2026</a></div></div></div> Mon, 02 Jun 2025 06:57:21 +0000 ruchi.singh@iisuniv.ac.in 1963 at https://chemistry.iisuniv.ac.in Environmental Chemistry https://chemistry.iisuniv.ac.in/courses/subjects/environmental-chemistry-17 <div class="field field-name-field-paper-code field-type-text field-label-inline clearfix"><div class="field-label">Paper Code: </div><div class="field-items"><div class="field-item even">25CHY325</div></div></div><div class="field field-name-field-credits field-type-text field-label-inline clearfix"><div class="field-label">Credits: </div><div class="field-items"><div class="field-item even">2</div></div></div><div class="field field-name-field-periods field-type-number-decimal field-label-inline clearfix"><div class="field-label">Contact Hours: </div><div class="field-items"><div class="field-item even">30.00</div></div></div><div class="field field-name-field-maxmarks field-type-number-decimal field-label-inline clearfix"><div class="field-label">Max. Marks: </div><div class="field-items"><div class="field-item even">100.00</div></div></div><div class="field field-name-field-objective field-type-text-long field-label-above"><div class="field-label">Objective: </div><div class="field-items"><div class="field-item even"><p><strong>This course will enable the students to </strong></p> <p>acquire the knowledge of the chemical and photochemical reactions essential for the emergence and existence of the cycling and accumulation of pollutants in the environment, to understand the chemistry of elements and compounds in the atmosphere and water, and know about the processes that define the connections and the dependence between individual segments of environment and sustainability.</p> <p> </p> </div></div></div><div class="field field-name-field-course-outcomes field-type-text-with-summary field-label-above"><div class="field-label">Course Outcomes: </div><div class="field-items"><div class="field-item even"><table border="1" cellpadding="0" cellspacing="0" id="tab" style="width: 100%" width="108%"> <thead> <tr> <th colspan="2" scope="col" style="width: 28.52%; height: 23px;"> <p><strong>Course</strong></p> </th> <th rowspan="2" scope="col" style="width: 31.26%; height: 23px;"> <p><strong>Learning outcome</strong></p> <p><strong>(at course level)</strong></p> </th> <th rowspan="2" scope="col" style="width: 21.66%; height: 23px;"> <p><strong>Learning and Teaching Strategies</strong></p> </th> <th rowspan="2" scope="col" style="width: 18.56%; height: 23px;"> <p><strong>Assessment Strategies </strong></p> </th> </tr> </thead> <tbody> <tr> <td style="width:11.3%;height:23px;"> <p align="center"><strong>Course Code</strong></p> </td> <td style="width:17.22%;height:23px;"> <p align="center"><strong>Course</strong></p> <p align="center"><strong>Title</strong></p> </td> </tr> <tr> <td style="width:11.3%;"> <p> </p> <p align="center"><strong>25CHY325</strong></p> </td> <td style="width:17.22%;"> <p align="center"> </p> <p align="center">Environmental Chemistry<strong> (Theory)</strong></p> </td> <td style="width:31.26%;"> <p style="margin-left:1.5pt;"><strong>CO 119:</strong> Discuss the concept of structure and function of different layers of the environment and issues related to them.</p> <p style="margin-left:1.5pt;"><strong>CO 120:</strong> Analyse the national and global environmental issues related to atmosphere, water and natural resources.</p> <p><strong>CO 121:</strong> Determine the range and extent of the water pollution with an understanding of some of the treatment procedures available.</p> <p style="margin-left:1.5pt;"><strong>CO 122:</strong> Identify relationships between chemical exposure and its effects on physiological system.</p> <p><strong>CO 123:</strong> Explain different natural resources, their management and conservation strategies.</p> <p style="margin-left:1.5pt;"><strong>CO 124:</strong> Contribute effectively in course-specific interaction.</p> </td> <td style="width:21.66%;"> <p><strong>Approach in teaching:</strong></p> <p>Interactive lectures, tutorials, group discussions and e-learning.</p> <p> </p> <p><strong>Learning activities for the students:</strong></p> <p>Peer learning, e- learning, problem solving through tutorials and group discussions.</p> <p> </p> <p> </p> </td> <td style="width:18.56%;"> <p>Written examinations,</p> <p>Assignments, Quiz</p> <p> </p> </td> </tr> </tbody> </table> <p> </p> </div></div></div><div class="field field-name-field-unit1hours field-type-number-decimal field-label-hidden"><div class="field-items"><div class="field-item even">7.00</div></div></div><div class="field field-name-field-unit1title field-type-text field-label-above"><div class="field-label">Unit I: </div><div class="field-items"><div class="field-item even"> General Aspects of Environmental Chemistry</div></div></div><div class="field field-name-field-unit1description field-type-text-long field-label-hidden"><div class="field-items"><div class="field-item even"><p>Atmosphere and its interaction with hydrosphere, lithosphere and biosphere, composition of air, water, soil.</p> <p>Atmospheric layers, vertical temperature profile, heat radiation budget of the earth atmosphere system. Properties of troposphere, thermodynamic derivation of lapse rate. Temperature inversion, pressure variation in atmosphere and scale height.</p> <p>Biogeochemical cycles of nitrogen and sulphur.</p> <p>Earth’s carbon cycle, carbon emitters, carbon sequestration, carbon footprint and carbon trading.</p> <p> </p> </div></div></div><div class="field field-name-field-unit2hours field-type-number-decimal field-label-hidden"><div class="field-items"><div class="field-item even">7.00</div></div></div><div class="field field-name-field-unit2title field-type-text field-label-above"><div class="field-label">Unit II: </div><div class="field-items"><div class="field-item even">Chemical and Photochemical Reactions in Atmosphere </div></div></div><div class="field field-name-field-unit2description field-type-text-long field-label-hidden"><div class="field-items"><div class="field-item even"><p> Formation and reactions of O<sub>3</sub>, O<sub>2</sub>, NO<sub>x</sub>, SO<sub>2</sub>, hydroxyl radical, hydroperoxyl radical, organic radicals, etc.</p> <p>Photochemical smog, green-house effect, ozone depletion and acid rain, effects and control of air pollutants-gaseous, particulates.</p> <p> </p> </div></div></div><div class="field field-name-field-unit3hours field-type-number-decimal field-label-hidden"><div class="field-items"><div class="field-item even">6.00</div></div></div><div class="field field-name-field-unit3title field-type-text field-label-above"><div class="field-label">Unit III: </div><div class="field-items"><div class="field-item even">Chemistry of Hydrosphere </div></div></div><div class="field field-name-field-unit3description field-type-text-long field-label-hidden"><div class="field-items"><div class="field-item even"><p>Chemical reactions in aquatic environment, concept of oxygen demand -DO, BOD, COD, TDS, pH, conductivity, colloids, salinity. Aquatic pollution- sources (inorganic and organic pollutants, pesticides, industrial effluents, sewage, detergents and oil spills), effect of pollutants on aquatic life (flora and fauna), purification and treatment of water.</p> <p> </p> <p> </p> </div></div></div><div class="field field-name-field-unit4hours field-type-number-decimal field-label-hidden"><div class="field-items"><div class="field-item even">5.00</div></div></div><div class="field field-name-field-unit4title field-type-text field-label-above"><div class="field-label">Unit IV: </div><div class="field-items"><div class="field-item even">Environmental Toxicology </div></div></div><div class="field field-name-field-unit4description field-type-text-long field-label-hidden"><div class="field-items"><div class="field-item even"><p>Toxicology: Threshold limiting value (TLV), LD50, toxicity and control of toxicants- nonmetallic compounds, asbestos, organic compounds (POP’s, phthalate, dioxins, PCB’s), pesticides, VOCs, endocrine disrupters.</p> <p> </p> </div></div></div><div class="field field-name-field-unit5hours field-type-number-decimal field-label-hidden"><div class="field-items"><div class="field-item even">5.00</div></div></div><div class="field field-name-field-unit5title field-type-text field-label-above"><div class="field-label">Unit V: </div><div class="field-items"><div class="field-item even">Renewable Energy </div></div></div><div class="field field-name-field-unit5description field-type-text-long field-label-hidden"><div class="field-items"><div class="field-item even"><p>Introduction, applications, merits and demerits of solar energy, biomass energy, hydrothermal energy, wind energy, geothermal energy and hydrogen fuel cells.</p> <p> </p> <p> </p> </div></div></div><div class="field field-name-field-essential-reading field-type-text-long field-label-above"><div class="field-label">Essential Readings: </div><div class="field-items"><div class="field-item even"><ol> <li>Environmental Chemistry, Tenth Edition; Stanley E. Manahan; CRC Press; 2017.</li> <li>Environmental Chemistry, Ninth Edition; A. K. De; New Age International Pvt. Ltd., New Delhi, 2018.</li> </ol> <p style="margin-left:.25in;"> </p> <p> </p> </div></div></div><div class="field field-name-field-references field-type-text-long field-label-above"><div class="field-label">References: </div><div class="field-items"><div class="field-item even"><ol> <li>Environmental Chemistry, Fifth Edition; Colin Baird; W.H. Freeman and company, New York, 2012.</li> <li>Chemistry of the Environment, Revised Third Edition; Thomas G. Spiro & William M. Stigliani; University Science Book, New Delhi, 2011.</li> </ol> <p style="margin-left:.25in;"> </p> <p style="margin-left:.25in;"><strong>e-Resources:</strong></p> <ol> <li><a href="https://nptel.ac.in/courses/104103020">https://nptel.ac.in/courses/104103020</a></li> <li><a href="https://epgp.inflibnet.ac.in/Home/ViewSubject?catid=13G8VouhmrFfuhs6rkiyTA==">https://epgp.inflibnet.ac.in/Home/ViewSubject?catid=13G8VouhmrFfuhs6rkiyTA==</a> (P-04)</li> <li><a href="https://cfpub.epa.gov/ecotox/search.cfm">https://cfpub.epa.gov/ecotox/search.cfm</a> (Environmental Toxicology)</li> </ol> <p> </p> <p style="margin-left:.25in;"> </p> <p> </p> </div></div></div><div class="field field-name-field-academic-year field-type-taxonomy-term-reference field-label-above"><div class="field-label">Academic Year: </div><div class="field-items"><div class="field-item even"><a href="/academic-year/2025-2026" typeof="skos:Concept" property="rdfs:label skos:prefLabel" datatype="">2025-2026</a></div></div></div> Mon, 02 Jun 2025 06:05:25 +0000 ruchi.singh@iisuniv.ac.in 1960 at https://chemistry.iisuniv.ac.in Spectroscopy III https://chemistry.iisuniv.ac.in/courses/subjects/spectroscopy-iii-0 <div class="field field-name-field-paper-code field-type-text field-label-inline clearfix"><div class="field-label">Paper Code: </div><div class="field-items"><div class="field-item even">25CHY324</div></div></div><div class="field field-name-field-credits field-type-text field-label-inline clearfix"><div class="field-label">Credits: </div><div class="field-items"><div class="field-item even">4</div></div></div><div class="field field-name-field-periods field-type-number-decimal field-label-inline clearfix"><div class="field-label">Contact Hours: </div><div class="field-items"><div class="field-item even">60.00</div></div></div><div class="field field-name-field-maxmarks field-type-number-decimal field-label-inline clearfix"><div class="field-label">Max. Marks: </div><div class="field-items"><div class="field-item even">100.00</div></div></div><div class="field field-name-field-objective field-type-text-long field-label-above"><div class="field-label">Objective: </div><div class="field-items"><div class="field-item even"><p><strong>This course will enable the students to </strong></p> <p>apprise with the instrumentation involved in the various spectroscopic techniques, understand and apply the key concepts of spectroscopy in the elucidation, characterization and inference of the relevant structural information of various known organic molecules.</p> <p> </p> </div></div></div><div class="field field-name-field-course-outcomes field-type-text-with-summary field-label-above"><div class="field-label">Course Outcomes: </div><div class="field-items"><div class="field-item even"><table border="1" cellpadding="0" cellspacing="0" id="tab" style="width: 100%" width="103%"> <thead> <tr> <th colspan="2" scope="col" style="width: 29.4%; height: 23px;"> <p><strong>Course</strong></p> </th> <th rowspan="2" scope="col" style="width: 32.18%; height: 23px;"> <p><strong>Learning outcome</strong></p> <p><strong>(at course level)</strong></p> </th> <th rowspan="2" scope="col" style="width: 21.06%; height: 23px;"> <p><strong>Learning and Teaching Strategies</strong></p> </th> <th rowspan="2" scope="col" style="width: 17.36%; height: 23px;"> <p><strong>Assessment Strategies </strong></p> </th> </tr> </thead> <tbody> <tr> <td style="width:12.48%;height:23px;"> <p align="center"><strong>Course Code</strong></p> </td> <td style="width:16.92%;height:23px;"> <p align="center"><strong>Course</strong></p> <p align="center"><strong>Title</strong></p> </td> </tr> <tr> <td style="width:12.48%;"> <p> </p> <p align="center"><strong>25CHY324</strong></p> </td> <td style="width:16.92%;"> <p align="center"> </p> <p align="center"><strong>Spectroscopy III</strong></p> <p align="center"><strong> (Theory)</strong></p> </td> <td style="width:32.18%;"> <p>CO113 Interpret the mass spectral data to identify  organic compounds.</p> <p>CO114 Calculate λmax and distinguish between the structures of simple compounds using Woodward-Feiser rules.</p> <p>CO115 Apply the principles of IR spectroscopy to identify the functional groups of compounds.</p> <p>CO116 Apply the principles of NMR to identify organic compounds.</p> <p><span style="font-family: "Helvetica Neue", Arial, Helvetica, sans-serif; font-size: 12.0012px;">CO117 </span>Employ the theoretical knowledge of techniques like COSY, NOSEY, HETCOR and DEPT along with 13C-NMR to identify the structures of compounds.</p> <p>C0118 Contribute effectively in course-specific interaction.</p> </td> <td style="width:21.06%;"> <p><strong>Approach in teaching:</strong></p> <p>Interactive lectures, tutorials, group discussions and e-learning.</p> <p> </p> <p><strong>Learning activities for the students:</strong></p> <p>Peer learning, e- learning, problem solving through tutorials and group discussions.</p> <p> </p> <p> </p> </td> <td style="width:17.36%;"> <p>Written examinations,</p> <p>Assignments, Quiz</p> <p> </p> </td> </tr> </tbody> </table> <p> </p> </div></div></div><div class="field field-name-field-unit1hours field-type-number-decimal field-label-hidden"><div class="field-items"><div class="field-item even">12.00</div></div></div><div class="field field-name-field-unit1title field-type-text field-label-above"><div class="field-label">Unit I: </div><div class="field-items"><div class="field-item even"> Mass Spectrometry</div></div></div><div class="field field-name-field-unit1description field-type-text-long field-label-hidden"><div class="field-items"><div class="field-item even"><p>Introduction, generation: EI, CI, HRMS, FD and FAB. Mass analyzer-electromagnetic field, quadrupole. Detection of molecular formula (HRMS) and determination of molecular formula, molecular ion, molecular ion peak, Nitrogen rule, isotope peak, metastable ions, Fragmentation- Basic fragmentation types and rules, factors influencing fragmentation, McLafferty rearrangement, fragmentation pattern of hydrocarbons, alcohols, ethers, ketones, aldehydes, carboxylic acids, amines, nitriles, nitro and halogenated compounds.</p> <p><strong>Self-Study: </strong>Problems of mass spectral fragmentation of organic compounds for structure determination.</p> <p> </p> </div></div></div><div class="field field-name-field-unit2hours field-type-number-decimal field-label-hidden"><div class="field-items"><div class="field-item even">12.00</div></div></div><div class="field field-name-field-unit2title field-type-text field-label-above"><div class="field-label">Unit II: </div><div class="field-items"><div class="field-item even">UV-Visible & Fluorescence Spectroscopy</div></div></div><div class="field field-name-field-unit2description field-type-text-long field-label-hidden"><div class="field-items"><div class="field-item even"><p>Electronic transitions (185-800 nm), Beer-Lambert rule, hypsochromic & bathochromic shifts, effect of conjugation, solvent effects, chromophores & auxochromes, characterization of organic compounds application of Woodward-Feiser rules to conjugated dienes, α,β- unsaturated  carbonyl  compounds,  benzene and benzene derivatives, polycyclic aromatic hydrocarbons, polyenes and polyenynes, steric effects in biphenyls and applications. An introduction to fluorescence spectroscopy.</p> <p> </p> </div></div></div><div class="field field-name-field-unit3hours field-type-number-decimal field-label-hidden"><div class="field-items"><div class="field-item even">10.00</div></div></div><div class="field field-name-field-unit3title field-type-text field-label-above"><div class="field-label">Unit III: </div><div class="field-items"><div class="field-item even">IR Spectroscopy </div></div></div><div class="field field-name-field-unit3description field-type-text-long field-label-hidden"><div class="field-items"><div class="field-item even"><p>Sampling, instrumentation and selection rules.</p> <p>Quantitative studies: Force constants, relation between force constant and vibrational frequencies, an introduction to near IR Overtones, combination bands and fermi-resonance, factors affecting the shift in group frequencies, isotope effect, hydrogen bonding, solvent effect, electronic effects (inductive and mesomeric) and steric effect, different absorption regions in IR spectrum and vibrational coupling.</p> <p>Characteristics functional group absorptions in organic compounds- carbon skeletal vibrations (alkanes, alkenes, alkynes, aromatic compounds), alcohols, phenols, ethers, ketones, aldehydes, carboxylic acids, amides, acid anhydrides, conjugated carbonyl compounds, esters, lactones, amines, amino acids (primary and secondary), interpretation of IR spectra of typical organic compounds.</p> <p> </p> </div></div></div><div class="field field-name-field-unit4hours field-type-number-decimal field-label-hidden"><div class="field-items"><div class="field-item even">12.00</div></div></div><div class="field field-name-field-unit4title field-type-text field-label-above"><div class="field-label">Unit IV: </div><div class="field-items"><div class="field-item even">Proton Magnetic Resonance Spectroscopy</div></div></div><div class="field field-name-field-unit4description field-type-text-long field-label-hidden"><div class="field-items"><div class="field-item even"><p>Nuclear properties, pulse technique, Fourier transform technique and its advantages, quantum number, chemical shift and factors affecting chemical shift, spin-spin interaction, factors affecting coupling constant, shielding mechanism, chemical shift values and correlation for protons bonded to carbon (aliphatic, olefinic, aldehydic and aromatic) and other nuclei (alcohols, phenols, enols, carboxylic acids, amines, amides and mercaptans), proton exchange, deuterium exchange, complex spin-spin interaction between two, three, four, and five nuclei (first order spectra).</p> <p>Hindered rotation, Karplus curve, variation of coupling constant with dihedral angle, simplification of complex spectra- nuclear magnetic double resonance, contact shift reagents, variable temperature dynamic NMR spectroscopy.</p> <p>Solvent effects, nuclear overhauser effect (NOE), a brief introduction of compounds carrying NMR active nuclei like 15N, 19F, 31P.</p> <p> </p> </div></div></div><div class="field field-name-field-unit5hours field-type-number-decimal field-label-hidden"><div class="field-items"><div class="field-item even">14.00</div></div></div><div class="field field-name-field-unit5title field-type-text field-label-above"><div class="field-label">Unit V: </div><div class="field-items"><div class="field-item even">13C and Advanced NMR Techniques and Combined Applications of Spectroscopic Techniques</div></div></div><div class="field field-name-field-unit5description field-type-text-long field-label-hidden"><div class="field-items"><div class="field-item even"><p>13C NMR spectroscopy: Basic principles, chemical shift, (aliphatic, olefinic, alkyne, aromatic, heteroaromatic & carbonyl carbon), proton (1H) coupled 13C NMR spectrum, off-resonance and noise decoupled 13C NMR spectrum, DEPT.</p> <p>2D-NMR spectroscopy: COSY, NOESY, HETCOR. Structure elucidation of organic compounds by combined application of UV, IR, NMR and mass spectroscopy.</p> <p> </p> </div></div></div><div class="field field-name-field-essential-reading field-type-text-long field-label-above"><div class="field-label">Essential Readings: </div><div class="field-items"><div class="field-item even"><ol> <li>Spectrometric Identification of Organic Compounds, Eighth Edition; R.M. Silverstein, F.X. Webster, David J. Kiemie and David L. Bryce; John Wiley and Sons, Inc., Singapore, 2014.</li> <li>Organic Spectroscopy, Third Edition; W. Kemp; Palgrave Publisher Ltd., New York, 2004.</li> </ol> <p style="margin-left:13.5pt;"> </p> <p> </p> <p align="left"> </p> <p> </p> </div></div></div><div class="field field-name-field-references field-type-text-long field-label-above"><div class="field-label">References: </div><div class="field-items"><div class="field-item even"><ol> <li>Spectroscopic Methods in Organic Chemistry; Sixth Edition; D. H. Williams and I. Fleming; Tata McGraw Hill Publishing Company Ltd, New Delhi, 2002.</li> <li>Structure Determination of Organic Compounds-Tables of Spectral Data; Fourth Edition; M. Badertscher, P. Bühlmann, E. Pretsch; Springer, Berlin, Heidelberg, 2009.</li> <li>Spectral Analysis of Organic Compounds; Second Edition; C.J. Creswell and M.M. Campbell; Burgess Publishing Company, Great Britain, 1972.</li> </ol> <p style="margin-left:13.5pt;"> </p> <p style="margin-left:13.5pt;"><strong>e-Resources:</strong></p> <ol> <li align="left"><a href="https://epgp.inflibnet.ac.in/Home/ViewSubject?catid=13G8VouhmrFfuhs6rkiyTA==">https://epgp.inflibnet.ac.in/Home/ViewSubject?catid=13G8VouhmrFfuhs6rkiyTA==</a>(Organic Spectroscopy)</li> <li><a href="https://www.youtube.com/watch?v=qqylkUqd12s">https://www.youtube.com/watch?v=qqylkUqd12s</a> (UV)</li> <li><a href="https://www.youtube.com/watch?v=_TmevMf-Zgs">https://www.youtube.com/watch?v=_TmevMf-Zgs</a> (IR )</li> <li><a href="https://nptel.ac.in/courses/104108078">https://nptel.ac.in/courses/104108078</a> (NMR)</li> <li><a href="https://nptel.ac.in/courses/104106075">https://nptel.ac.in/courses/104106075</a> (NMR)</li> <li><a href="https://www.youtube.com/watch?v=SBir5wUS3Bo">https://www.youtube.com/watch?v=SBir5wUS3Bo</a> (NMR)</li> <li><a href="https://www.youtube.com/watch?v=hSirWciIvSg">https://www.youtube.com/watch?v=hSirWciIvSg</a> (Mass)</li> </ol> <p> </p> <p> </p> <p> </p> </div></div></div><div class="field field-name-field-academic-year field-type-taxonomy-term-reference field-label-above"><div class="field-label">Academic Year: </div><div class="field-items"><div class="field-item even"><a href="/academic-year/2025-2026" typeof="skos:Concept" property="rdfs:label skos:prefLabel" datatype="">2025-2026</a></div></div></div> Mon, 02 Jun 2025 05:45:51 +0000 ruchi.singh@iisuniv.ac.in 1955 at https://chemistry.iisuniv.ac.in Electrochemistry and Chemical Kinetics https://chemistry.iisuniv.ac.in/courses/subjects/electrochemistry-and-chemical-kinetics-16 <div class="field field-name-field-paper-code field-type-text field-label-inline clearfix"><div class="field-label">Paper Code: </div><div class="field-items"><div class="field-item even">25CHY323</div></div></div><div class="field field-name-field-credits field-type-text field-label-inline clearfix"><div class="field-label">Credits: </div><div class="field-items"><div class="field-item even">4</div></div></div><div class="field field-name-field-periods field-type-number-decimal field-label-inline clearfix"><div class="field-label">Contact Hours: </div><div class="field-items"><div class="field-item even">60.00</div></div></div><div class="field field-name-field-maxmarks field-type-number-decimal field-label-inline clearfix"><div class="field-label">Max. Marks: </div><div class="field-items"><div class="field-item even">100.00</div></div></div><div class="field field-name-field-objective field-type-text-long field-label-above"><div class="field-label">Objective: </div><div class="field-items"><div class="field-item even"><p><strong>This course will enable the students to </strong></p> <p>aware about the behaviour of ions in solution and structure of electrode surface and learn about the rate laws from a proposed mechanism and analyze kinetics in gases and solutions.</p> <p> </p> </div></div></div><div class="field field-name-field-course-outcomes field-type-text-with-summary field-label-above"><div class="field-label">Course Outcomes: </div><div class="field-items"><div class="field-item even"><table border="1" cellpadding="0" cellspacing="0" id="tab" style="width: 100%" width="103%"> <thead> <tr> <th colspan="2" scope="col" style="width: 33.34%; height: 23px;"> <p><strong>Course</strong></p> </th> <th rowspan="2" scope="col" style="width: 24.26%; height: 23px;"> <p><strong>Learning outcome</strong></p> <p><strong>(at course level)</strong></p> </th> <th rowspan="2" scope="col" style="width: 22.86%; height: 23px;"> <p><strong>Learning and Teaching Strategies</strong></p> </th> <th rowspan="2" scope="col" style="width: 19.54%; height: 23px;"> <p><strong>Assessment Strategies </strong></p> </th> </tr> </thead> <tbody> <tr> <td style="width:11.86%;height:23px;"> <p align="center"><strong>Course Code</strong></p> </td> <td style="width:21.48%;height:23px;"> <p align="center"><strong>Course</strong></p> <p align="center"><strong>Title</strong></p> </td> </tr> <tr> <td style="width:11.86%;"> <p> </p> <p align="center"><strong>25CHY323</strong></p> </td> <td style="width:21.48%;"> <p align="center"> </p> <p align="center"><strong>Electrochemistry and Chemical Kinetics </strong></p> <p align="center"><strong>(Theory)</strong></p> </td> <td style="width:24.26%;"> <p>CO107 Explain different theories to understand the behavior of strong electrolytes.</p> <p>CO108 Interpret the structure and nature of electrical double layer and describe electro kinetic phenomena.</p> <p>CO109 Explain kinetics of electrode reactions with the help of Butler-Volmer equation and Tafel equation.</p> <p>CO110 Describe theories of chemical kinetics to understand rate law for chemical reaction and discuss salt effect.</p> <p>CO111 Determine rate law for a complex reaction using steady state approximation.</p> <p>CO112 Contribute effectively in course-specific interaction.</p> </td> <td style="width:22.86%;"> <p><strong>Approach in teaching:</strong></p> <p>Interactive lectures, tutorials, group discussions and e-learning.</p> <p> </p> <p><strong>Learning activities for the students:</strong></p> <p>Peer learning, e- learning, problem solving through tutorials and group discussions.</p> <p> </p> <p> </p> </td> <td style="width:19.54%;"> <p>Written examinations,</p> <p>Assignments, Quiz</p> <ul> <li align="left"> </li> </ul> </td> </tr> </tbody> </table> <p> </p> </div></div></div><div class="field field-name-field-unit1hours field-type-number-decimal field-label-hidden"><div class="field-items"><div class="field-item even">10.00</div></div></div><div class="field field-name-field-unit1title field-type-text field-label-above"><div class="field-label">Unit I: </div><div class="field-items"><div class="field-item even"> Ions in Solution</div></div></div><div class="field field-name-field-unit1description field-type-text-long field-label-hidden"><div class="field-items"><div class="field-item even"><p>Debye Huckel theory of strong electrolytes, Debye Huckel Onsager equation, activity coefficient, mean ionic activity coefficient, physical significance of activity coefficients, mean activity coefficient of an electrolyte and its determination, ionic strength, Debye Huckel theory of mean ionic activity coefficient, Debye-Huckel limiting law, qualitative and quantitative verification of Debye-Huckel limiting law, Debye length, ionic strength, Bjerrum model of ion-association.</p> <p style="margin-left:30.0pt;"> </p> <p> </p> </div></div></div><div class="field field-name-field-unit2hours field-type-number-decimal field-label-hidden"><div class="field-items"><div class="field-item even">12.00</div></div></div><div class="field field-name-field-unit2title field-type-text field-label-above"><div class="field-label">Unit II: </div><div class="field-items"><div class="field-item even">Electrochemistry: Electrical Double Layer</div></div></div><div class="field field-name-field-unit2description field-type-text-long field-label-hidden"><div class="field-items"><div class="field-item even"><p>Introduction, evidences and structure of electrical double layer- Helmholtz-Perrin, Guoy-Chapman, Stern theory, measurement of zeta potential (electrokinetic phenomena), influence of ions on electrokinetic phenomena, electro capillary phenomenon: Electro capillary curves, Lipmann’s equation.</p> <p>Graham, Devanathan, Mottwatts-Tobin, Bockris-Devanathan-Müller models. Quantum aspects of charge transfer at electrodes-solution interfaces, tunneling.</p> </div></div></div><div class="field field-name-field-unit3hours field-type-number-decimal field-label-hidden"><div class="field-items"><div class="field-item even">12.00</div></div></div><div class="field field-name-field-unit3title field-type-text field-label-above"><div class="field-label">Unit III: </div><div class="field-items"><div class="field-item even">Kinetics of Electrode Reactions</div></div></div><div class="field field-name-field-unit3description field-type-text-long field-label-hidden"><div class="field-items"><div class="field-item even"><p>Electrodics of elementary electrode reactions- determination of anode and cathode potential, decomposition voltage of electrolyte, diffusion over potential, hydrogen and oxygen over voltage, influence of various factors on over voltage, theoretical investigation of kinetics of an electrode reaction- standard rate constant (k<sup>0</sup>) and transfer coefficient (α), exchange current, Butler-Volmer equation, Tafel equation. Electrocatalysis- introduction and influence of various parameters.</p> <p>Semiconductor solution interfaces, effect of light at semiconductor solution interface.</p> <p> </p> </div></div></div><div class="field field-name-field-unit4hours field-type-number-decimal field-label-hidden"><div class="field-items"><div class="field-item even">13.00</div></div></div><div class="field field-name-field-unit4title field-type-text field-label-above"><div class="field-label">Unit IV: </div><div class="field-items"><div class="field-item even">Statistical Theories of Kinetics</div></div></div><div class="field field-name-field-unit4description field-type-text-long field-label-hidden"><div class="field-items"><div class="field-item even"><p>Collision theory of reaction rates, steric factor, activated complex theory, comparison between collision theory and activated-complex theory. Unimolecular gas reactions- dynamics of unimolecular reactions (Lindemann, Hinshelwood, RRK and RRKM theories), primary and secondary salt effects- influence of ionic strength and dielectric constant on reactions involving (i) ions (ii) dipoles (iii) ion and dipole.</p> <p> </p> </div></div></div><div class="field field-name-field-unit5hours field-type-number-decimal field-label-hidden"><div class="field-items"><div class="field-item even">13.00</div></div></div><div class="field field-name-field-unit5title field-type-text field-label-above"><div class="field-label">Unit V: </div><div class="field-items"><div class="field-item even">Complex Reactions </div></div></div><div class="field field-name-field-unit5description field-type-text-long field-label-hidden"><div class="field-items"><div class="field-item even"><p>Equilibrium and steady state approximation and their application in reaction mechanisms, rate expression for opposing, parallel and consecutive reactions, kinetic and thermodynamic control of the reactions, chain reactions- Thermal and photochemical reactions, dynamic chain (mechanism of hydrogen-bromine and hydrogen-chlorine reactions), decomposition of ethane, pyrolysis of acetaldehyde, oscillatory reactions: Belousov-Zhabotinsky reaction.</p> <p> </p> </div></div></div><div class="field field-name-field-essential-reading field-type-text-long field-label-above"><div class="field-label">Essential Readings: </div><div class="field-items"><div class="field-item even"><ol> <li>An Introduction to Electrochemistry; Seventh Edition; S. Glasstone, East-West press Pvt. Ltd., New Delhi, 2016.</li> <li>Chemical Kinetics, Third Edition; K.J. Laidler; Pearson Education Pvt. Ltd., Singapore, 2013.</li> </ol> <p style="margin-left:.25in;"> </p> <p> </p> </div></div></div><div class="field field-name-field-references field-type-text-long field-label-above"><div class="field-label">References: </div><div class="field-items"><div class="field-item even"><ol> <li>Modern Electrochemistry Vol. I, II A & II B, Second Edition; J. O’M. Bockris and K.N. Reddy; Kluwer Academic Publishers, New York, 2001.</li> <li>Electrochemistry- Principles, Methods and Applications; First edition, C. M. A. Brett and A. M. O. Brett; Oxford University Press, Great Britain, 1994.</li> <li>Kinetics and Mechanisms of Chemical Transformations, First Edition; J. Rajaram and J.C. Kuriacose; Macmillan Publisher India Ltd., New Delhi, 2011.</li> <li>Advanced Physical Chemistry, Eighteenth Edition; J. N. Gurtu and A. Gurtu, Pragati Prakashan, Meerut 2015.</li> </ol> <p style="margin-left:.25in;"> </p> <p style="margin-left:.25in;">e-Resources:</p> <ol> <li><a href="https://nptel.ac.in/courses/104106129">https://nptel.ac.in/courses/104106129</a></li> <li><a href="https://nptel.ac.in/courses/104101128">https://nptel.ac.in/courses/104101128</a></li> <li><a href="https://archive.nptel.ac.in/courses/104/101/104101128/">https://archive.nptel.ac.in/courses/104/101/104101128/</a></li> <li><a href="https://www.youtube.com/watch?v=ibG2TrqbQ0g">https://www.youtube.com/watch?v=ibG2TrqbQ0g</a></li> </ol> <p> </p> </div></div></div><div class="field field-name-field-academic-year field-type-taxonomy-term-reference field-label-above"><div class="field-label">Academic Year: </div><div class="field-items"><div class="field-item even"><a href="/academic-year/2025-2026" typeof="skos:Concept" property="rdfs:label skos:prefLabel" datatype="">2025-2026</a></div></div></div> Mon, 02 Jun 2025 05:40:29 +0000 ruchi.singh@iisuniv.ac.in 1954 at https://chemistry.iisuniv.ac.in Organometallic Chemistry https://chemistry.iisuniv.ac.in/courses/subjects/organometallic-chemistry-7 <div class="field field-name-field-paper-code field-type-text field-label-inline clearfix"><div class="field-label">Paper Code: </div><div class="field-items"><div class="field-item even">25CHY322</div></div></div><div class="field field-name-field-credits field-type-text field-label-inline clearfix"><div class="field-label">Credits: </div><div class="field-items"><div class="field-item even">4</div></div></div><div class="field field-name-field-periods field-type-number-decimal field-label-inline clearfix"><div class="field-label">Contact Hours: </div><div class="field-items"><div class="field-item even">60.00</div></div></div><div class="field field-name-field-maxmarks field-type-number-decimal field-label-inline clearfix"><div class="field-label">Max. Marks: </div><div class="field-items"><div class="field-item even">100.00</div></div></div><div class="field field-name-field-objective field-type-text-long field-label-above"><div class="field-label">Objective: </div><div class="field-items"><div class="field-item even"><p><strong>This course will enable the students to </strong></p> <p>develop a vast knowledge about different reactions leading to the formation of various organometallic complexes and the mechanism involved in homo- and heterogeneous catalysis, learn about the various applications of organometallic complexes in catalysis and get acquainted them with the promising future of organo-transition metal chemistry in industrial, biological and environmental fields.</p> <p> </p> </div></div></div><div class="field field-name-field-course-outcomes field-type-text-with-summary field-label-above"><div class="field-label">Course Outcomes: </div><div class="field-items"><div class="field-item even"><table border="1" cellpadding="0" cellspacing="0" id="tab" style="width: 100%" width="103%"> <thead> <tr> <th colspan="2" scope="col" style="width: 31.68%; height: 23px;"> <p align="center"><strong>Course</strong></p> </th> <th rowspan="2" scope="col" style="width: 30.94%; height: 23px;"> <p><strong>Learning outcome</strong></p> <p><strong>(at course level)</strong></p> </th> <th rowspan="2" scope="col" style="width: 21.24%; height: 23px;"> <p><strong>Learning and Teaching Strategies</strong></p> </th> <th rowspan="2" scope="col" style="width: 16.14%; height: 23px;"> <p><strong>Assessment Strategies </strong></p> </th> </tr> </thead> <tbody> <tr> <td style="width:13.66%;height:23px;"> <p align="center"><strong>Course Code</strong></p> </td> <td style="width:18.02%;height:23px;"> <p align="center"><strong>Course</strong></p> <p align="center"><strong>Title</strong></p> </td> </tr> <tr> <td style="width:13.66%;"> <p> </p> <p align="center"><strong>25CHY322</strong></p> </td> <td style="width:18.02%;"> <p align="center"> </p> <p align="center">Organometallic Chemistry<strong> (Theory)</strong></p> </td> <td style="width:30.94%;"> <p>CO101 Classify organometallic compounds, calculate valence electron counts, discuss routes of synthesis and decomposition pathways of organometallic compounds.</p> <p>CO102 Discuss preparation, properties, structure, bonding of carbene and carbyne complexes</p> <p>CO103 Discuss the properties, structure and bonding of M-C multiple bonded organometallic compounds.</p> <p>CO104 Describe and identify the reaction mechanisms of various homogeneous and heterogenous catalysts.</p> <p>CO105 Explain structure, bonding and properties of metal carbonyls, dinitrogen and dioxygen complexes, differentiate between terminal and bridging carbonyls and interpret the type of bonding on the basis of IR spectra.</p> <p>CO106 Contribute effectively in course-specific interaction.</p> </td> <td style="width:21.24%;"> <p><strong>Approach in teaching:</strong></p> <p>Interactive lectures, tutorials, group discussions and e-learning.</p> <p> </p> <p><strong>Learning activities for the students:</strong></p> <p>Peer learning, e- learning, problem solving through tutorials and group discussions.</p> <p> </p> <p> </p> </td> <td style="width:16.14%;"> <p>Written examinations,</p> <p>Assignments,</p> <p>Quiz</p> <ul> <li align="left"> </li> </ul> </td> </tr> </tbody> </table> <p> </p> </div></div></div><div class="field field-name-field-unit1hours field-type-number-decimal field-label-hidden"><div class="field-items"><div class="field-item even">10.00</div></div></div><div class="field field-name-field-unit1title field-type-text field-label-above"><div class="field-label">Unit I: </div><div class="field-items"><div class="field-item even"> Introduction to Organometallic Compounds </div></div></div><div class="field field-name-field-unit1description field-type-text-long field-label-hidden"><div class="field-items"><div class="field-item even"><p>Types of transition metal to carbon bonds, classification of organometallic compounds </p> <p>based on hapticity and polarity of M-C bond, nomenclature and general characteristics, electron counting (16 and 18 electron rules), routes of synthesis for s-alkyls and aryls of transition metals, stability of organometallic compounds and decomposition pathways.</p> <p> </p> </div></div></div><div class="field field-name-field-unit2hours field-type-number-decimal field-label-hidden"><div class="field-items"><div class="field-item even">10.00</div></div></div><div class="field field-name-field-unit2title field-type-text field-label-above"><div class="field-label">Unit II: </div><div class="field-items"><div class="field-item even">Metal-Carbon Multiple Bonded Organometallics-I </div></div></div><div class="field field-name-field-unit2description field-type-text-long field-label-hidden"><div class="field-items"><div class="field-item even"><p>Preparation, properties, structure and bonding of carbene and carbyne complexes (both Fischer and Schrock types), nucleophilic and electrophilic reactions on the ligands, role in organic synthesis.         </p> </div></div></div><div class="field field-name-field-unit3hours field-type-number-decimal field-label-hidden"><div class="field-items"><div class="field-item even">13.00</div></div></div><div class="field field-name-field-unit3title field-type-text field-label-above"><div class="field-label">Unit III: </div><div class="field-items"><div class="field-item even">Metal-Carbon Multiple Bonded Organometallics-II</div></div></div><div class="field field-name-field-unit3description field-type-text-long field-label-hidden"><div class="field-items"><div class="field-item even"><p>Preparation, properties, structure and bonding of h<sup>4</sup>- diene complexes, h<sup>5</sup>- dienyl    </p> <p>complexes, h<sup>6</sup>- arene complexes,fluxionality and dynamic equilibria in such as h<sup>2</sup>- olefin,  h<sup>3</sup> allyl and h<sup>5-</sup>dienyl complexes.</p> <p> </p> </div></div></div><div class="field field-name-field-unit4hours field-type-number-decimal field-label-hidden"><div class="field-items"><div class="field-item even">15.00</div></div></div><div class="field field-name-field-unit4title field-type-text field-label-above"><div class="field-label">Unit IV: </div><div class="field-items"><div class="field-item even">Catalysis by Organotransition Metal Complexes</div></div></div><div class="field field-name-field-unit4description field-type-text-long field-label-hidden"><div class="field-items"><div class="field-item even"><p>Principles and important reactions of transition metal organometallics: Co-coordinative unsaturation, oxidative addition, insertion and product isolation(reductive elimination and β- elimination).</p> <p>Homogeneous catalysis: Hydrogenation of alkenes, hydrosilylation of alkenes, metathesis of alkenes, oligomerization and polymerization of alkenes and alkynes, hydroformylation of alkenes, acetic acid synthesis and other carbonylation reactions, oxidation reactions of alkenes.</p> <p>Heterogeneous catalysis: Fischer Tropsch process- Methanation reaction, synthesis of methanol, gasoline  production, water gas shift reaction, role of ZnO/Cr<sub>2</sub>O<sub>3</sub> in the reaction, acetic acid synthesis, role of CO catalyst.</p> <p> </p> </div></div></div><div class="field field-name-field-unit5hours field-type-number-decimal field-label-hidden"><div class="field-items"><div class="field-item even">12.00</div></div></div><div class="field field-name-field-unit5title field-type-text field-label-above"><div class="field-label">Unit V: </div><div class="field-items"><div class="field-item even">Metal π-Complexes </div></div></div><div class="field field-name-field-unit5description field-type-text-long field-label-hidden"><div class="field-items"><div class="field-item even"><p>Metal carbonyls: Preparation, properties, structure and bonding with special reference to dinuclear and polynuclear carbonyls, vibrational spectra of metal carbonyls (bridging and terminal) for bonding and structural elucidation, metal carbonyl clusters.</p> <p>Dinitrogen and dioxygen complexes: Preparation, properties, structure and bonding.</p> <p> </p> </div></div></div><div class="field field-name-field-essential-reading field-type-text-long field-label-above"><div class="field-label">Essential Readings: </div><div class="field-items"><div class="field-item even"><ol> <li>Organometallic Chemistry: A Unified Approach, Second Edition; R.C. Mehrotra, A.Singh; New Age International Private Limited, New Delhi, 2000.</li> <li>Inorganic Chemistry, Fifth Edition; G. L. Miessler, D. A. Tarr; Pearson Education Inc. Singapore, 2013.</li> <li>Inorganic Chemistry (Principle of Structure and Reactivity), Fourth Edition; J. E Huheey, E. A. Keiter, R. L. Keiter; Pearson India, New Delhi, 2013</li> </ol> <p style="margin-left:.25in;"> </p> <p> </p> </div></div></div><div class="field field-name-field-references field-type-text-long field-label-above"><div class="field-label">References: </div><div class="field-items"><div class="field-item even"><ol> <li>The Organometallic Chemistry of the Transition Metals, Fourth Edition; R. H. Crabtree;  John Wiley and Sons, Inc., New Jersey, 2005.</li> <li>Advanced Inorganic Chemistry, Sixth Edition; F.A. Cotton, G. Wilkinson, C.A. Murillo, M. Bochmann; John Wiley and Sons, USA, New York, 2007.</li> </ol> <p style="margin-left:.25in;"> </p> <p style="margin-left:.25in;"><strong>e-Resources:</strong></p> <p align="left">1.    <a href="https://nptel.ac.in/courses/104101079">https://nptel.ac.in/courses/104101079</a></p> <p align="left">2.    <a href="https://nptel.ac.in/courses/104101091">https://nptel.ac.in/courses/104101091</a></p> <p align="left">3.    <a href="https://epgp.inflibnet.ac.in/Home/ViewSubject?catid=13G8VouhmrFfuhs6rkiyTA==">https://epgp.inflibnet.ac.in/Home/ViewSubject?catid=13G8VouhmrFfuhs6rkiyTA==</a>  (P11)</p> <p> </p> </div></div></div><div class="field field-name-field-academic-year field-type-taxonomy-term-reference field-label-above"><div class="field-label">Academic Year: </div><div class="field-items"><div class="field-item even"><a href="/academic-year/2025-2026" typeof="skos:Concept" property="rdfs:label skos:prefLabel" datatype="">2025-2026</a></div></div></div> Mon, 02 Jun 2025 05:33:59 +0000 ruchi.singh@iisuniv.ac.in 1951 at https://chemistry.iisuniv.ac.in Photochemistry, Pericyclic Reactions and Disconnection Approach https://chemistry.iisuniv.ac.in/courses/subjects/photochemistry-pericyclic-reactions-and-disconnection-approach-2 <div class="field field-name-field-paper-code field-type-text field-label-inline clearfix"><div class="field-label">Paper Code: </div><div class="field-items"><div class="field-item even">25CHY321</div></div></div><div class="field field-name-field-credits field-type-text field-label-inline clearfix"><div class="field-label">Credits: </div><div class="field-items"><div class="field-item even">4</div></div></div><div class="field field-name-field-periods field-type-number-decimal field-label-inline clearfix"><div class="field-label">Contact Hours: </div><div class="field-items"><div class="field-item even">60.00</div></div></div><div class="field field-name-field-maxmarks field-type-number-decimal field-label-inline clearfix"><div class="field-label">Max. Marks: </div><div class="field-items"><div class="field-item even">100.00</div></div></div><div class="field field-name-field-objective field-type-text-long field-label-above"><div class="field-label">Objective: </div><div class="field-items"><div class="field-item even"><p><strong>This course will enable the students to </strong></p> <p>acquire in-depth knowledge of various photochemical reactions and their basic principles which enables students to learn a variety of photochemical reactions, and their mechanisms and understand the various organic transformations through the disconnection approach.</p> <p> </p> </div></div></div><div class="field field-name-field-course-outcomes field-type-text-with-summary field-label-above"><div class="field-label">Course Outcomes: </div><div class="field-items"><div class="field-item even"><table border="1" cellpadding="0" cellspacing="0" id="tab" style="width: 100%" width="102%"> <thead> <tr> <th colspan="2" scope="col" style="width: 34.92%; height: 23px;"> <p align="center"><strong>Course</strong></p> </th> <th rowspan="2" scope="col" style="width: 29.22%; height: 23px;"> <p><strong>Learning outcome</strong></p> <p><strong>(at course level)</strong></p> </th> <th rowspan="2" scope="col" style="width: 21.14%; height: 23px;"> <p><strong>Learning and Teaching Strategies</strong></p> </th> <th rowspan="2" scope="col" style="width: 14.72%; height: 23px;"> <p><strong>Assessment Strategies </strong></p> </th> </tr> </thead> <tbody> <tr> <td style="width:11.96%;height:23px;"> <p align="center"><strong>Course Code</strong></p> </td> <td style="width:22.96%;height:23px;"> <p align="center"><strong>Course</strong></p> <p align="center"><strong>Title</strong></p> </td> </tr> <tr> <td style="width:11.96%;"> <p> </p> <p align="center"><strong>25CHY321</strong></p> </td> <td style="width:22.96%;"> <p align="center"> </p> <p align="center">Photochemistry, Pericyclic Reactions and Disconnection Approach</p> <p align="center"><strong>(Theory)</strong></p> </td> <td style="width:29.22%;"> <p>CO95 Distinguish between thermal and photochemical reactions and explain the photochemistry of carbonyl compounds.</p> <p>CO96 Explain the various photochemical reactions of alkenes and aromatic compounds along with singlet oxygen reactions.</p> <p>CO97 Appraise the orbital interactions and orbital symmetry correlations in electrocyclic reactions to solve various problems.</p> <p>C098 Explain and justify pericyclic reactions and their products in cycloaddition and sigmatropic reactions.</p> <p>C099 Justify retrosynthetic methods for the logical dissection of complex organic molecules and devise appropriate routes for their synthesis. Predict logical uses of various reagents in organic synthesis.</p> <p>CO100 Contribute effectively in course-specific interaction.</p> </td> <td style="width:21.14%;"> <p><strong>Approach in teaching:</strong></p> <p>Interactive lectures, tutorials, group discussions and e-learning.</p> <p> </p> <p><strong>Learning activities for the students:</strong></p> <p>Peer learning, e- learning, problem solving through tutorials and group discussions.</p> <p> </p> <p> </p> </td> <td style="width:14.72%;"> <p>Written examinations,</p> <p>Assignments, Quiz</p> <p> </p> </td> </tr> </tbody> </table> <p> </p> </div></div></div><div class="field field-name-field-unit1hours field-type-number-decimal field-label-hidden"><div class="field-items"><div class="field-item even">12.00</div></div></div><div class="field field-name-field-unit1title field-type-text field-label-above"><div class="field-label">Unit I: </div><div class="field-items"><div class="field-item even"> Basics of Photochemistry and Photochemical Reactions of Carbonyl Compounds</div></div></div><div class="field field-name-field-unit1description field-type-text-long field-label-hidden"><div class="field-items"><div class="field-item even"><p>Laws of photochemistry. Fate of excited molecules: Jablonski diagram, intersystem crossing, energy transfer, photosensitization, quenching, quantum yield, Stern-Volmer equation. Photochemical reactions of ketones – alpha cleavage or Norrish type I cleavage, gamma hydrogen transfer or Norrish type II cleavage; photo reductions; Paterno-Buchi reactions; Photochemistry  of  α,β-unsaturated  ketones,  β,γ-unsaturated  ketones,  cyclohexadienones (cross conjugated and conjugated).</p> <p> </p> </div></div></div><div class="field field-name-field-unit2hours field-type-number-decimal field-label-hidden"><div class="field-items"><div class="field-item even">10.00</div></div></div><div class="field field-name-field-unit2title field-type-text field-label-above"><div class="field-label">Unit II: </div><div class="field-items"><div class="field-item even">Photochemistry of Alkenes and Aromatic Compounds </div></div></div><div class="field field-name-field-unit2description field-type-text-long field-label-hidden"><div class="field-items"><div class="field-item even"><p>Photochemistry of alkenes: Intramolecular reactions of the olefinic bond, cis<strong>-</strong>trans isomerisation (stilbene), cyclization reactions, rearrangement of 1,4 and 1,5-dienes, di-π methanerearrangement.</p> <p>Photochemistry of aromatic compounds: Photochemical rearrangement, photostationary state, 1, 3, 5 – trimethyl benzene to 1, 2, 4-trimethyl benzene.</p> <p>Miscellaneous Photochemical Reactions<strong>- </strong>Barton reaction, photo Fries rearrangement of ethers and anilides, singlet oxygen reactions (photo oxygenation).</p> <p> </p> </div></div></div><div class="field field-name-field-unit3hours field-type-number-decimal field-label-hidden"><div class="field-items"><div class="field-item even">10.00</div></div></div><div class="field field-name-field-unit3title field-type-text field-label-above"><div class="field-label">Unit III: </div><div class="field-items"><div class="field-item even">Pericyclic Reactions -I</div></div></div><div class="field field-name-field-unit3description field-type-text-long field-label-hidden"><div class="field-items"><div class="field-item even"><p>General characteristics, classification, molecular orbital symmetry.</p> <p>Electrocyclic reactions: Theories of explanation (FMO, Woodward-Hoffmann and PMO approach), frontier orbitals, electrocyclisation and reterocyclisation of 1,3 butadiene, cyclobutadiene and ,hexatriene derivatives, allylic cations(1,5 diphenylpentadienyl cation) and allylic anions (1,5 diphenylpentadienyl anion), ring opening in bicyclo [4.1.0] heptane derivatives, valence tautomerism.</p> <p> </p> </div></div></div><div class="field field-name-field-unit4hours field-type-number-decimal field-label-hidden"><div class="field-items"><div class="field-item even">10.00</div></div></div><div class="field field-name-field-unit4title field-type-text field-label-above"><div class="field-label">Unit IV: </div><div class="field-items"><div class="field-item even">Pericyclic Reactions–II</div></div></div><div class="field field-name-field-unit4description field-type-text-long field-label-hidden"><div class="field-items"><div class="field-item even"><p>Cycloaddition reactions: 2+2, 4+2 cycloaddition, 1, 3-dipolar cycloaddition and cheletropic reactions, stereoselectivity (endo, exo), stereospecific and regioselective hydrogen reactions, Lewis-acid catalysis in Diels- Alder reaction.</p> <p>Sigmatropic rearrangements: Suprafacial and antarafacial shifts of H , sigmatropic shifts involving carbon moieties, 3, 3- and 5, 5-sigmatropic rearrangements, Claisen, Cope and Aza- Cope rearrangements, isomerization of divinyl cyclopropane, Fluxional tautomerism (bullvalene), Ene reaction.</p> <p> </p> </div></div></div><div class="field field-name-field-unit5hours field-type-number-decimal field-label-hidden"><div class="field-items"><div class="field-item even">18.00</div></div></div><div class="field field-name-field-unit5title field-type-text field-label-above"><div class="field-label">Unit V: </div><div class="field-items"><div class="field-item even">Disconnection Approach in Organic Synthesis</div></div></div><div class="field field-name-field-unit5description field-type-text-long field-label-hidden"><div class="field-items"><div class="field-item even"><p>Disconnection approach, Synthons and synthetic equivalents, d, d, dand dsynthons, , functional group inter-conversions, the importance of the order of events in organic synthesis, one group C-X and two group C-X disconnections, chemoselectivity, reversal of polarity, cyclisation reactions, amine synthesis, principle of protection of alcohol, amine, carbonyl and carboxylgroups.</p> <h2><span style="font-size:10px;"><strong>One and Two Group C-C Disconnections</strong></span></h2> <p>Alcohols and carbonyl compounds, regioselectivity, alkene synthesis, uses of alkynes and aliphatic nitro compounds in organic synthesis, Diels- Alder reaction, 1,3-difunctionalised compounds, α, β-unsaturated carbonyl compounds, control in carbonyl condensations, 1,5- difunctionalised compounds, Michael addition and Robinson annelation.</p> <p> </p> </div></div></div><div class="field field-name-field-essential-reading field-type-text-long field-label-above"><div class="field-label">Essential Readings: </div><div class="field-items"><div class="field-item even"><ol> <li>Fundamentals of Photochemistry, Third Edition; K.K. Rohatagi and Mukherjee; New Age International Publishers Pvt. Ltd., New Delhi, 2007.</li> <li>Reaction Mechanism in Organic Chemistry, Third Edition; S.M. Mukherjee and S.P. Singh; Macmillan, India Ltd., New Delhi, 2003.</li> <li>Modern Methods of Organic Synthesis, Fourth Edition; W. Carruthers; Cambridge Univ. Press, UK, 2005.</li> </ol> <p> </p> </div></div></div><div class="field field-name-field-references field-type-text-long field-label-above"><div class="field-label">References: </div><div class="field-items"><div class="field-item even"><ol> <li>CRC Handbook of Organic Photochemistry and Photobiology, Second Edition; W. Horspool and</li> <li>F. Lenci; CRC Press LLC, US, 2004.</li> <li>Molecular Reactions and Photochemistry, First Edition, C. H. Depuy and L. Orville Chapman; Prentice-Hall of India Pvt. Ltd, New Delhi, 1988.</li> <li>Advanced Organic Chemistry Part A & B, Fifth Edition; F. A. Carey and R. J. Sundberg; Springer, US, 2007.</li> <li>Designing Organic Synthesis: A Programmed Introduction to the Sython Approach, First Edition; S. Warren; John Wiley and Sons, Great Britain, 2010.</li> <li>Organic Synthesis- Concepts, Methods and Starting Materials, J. Fuhrhop and G.Penzillin; Second Edition; Wiley-VCH, New York: 2003.</li> </ol> <p style="margin-left:.25in;"> </p> <p style="margin-left:.25in;"><strong>e-Resources:</strong></p> <ol> <li><a href="https://epgp.inflibnet.ac.in/Home/ViewSubject?catid=13G8VouhmrFfuhs6rkiyTA==">https://epgp.inflibnet.ac.in/Home/ViewSubject?catid=13G8VouhmrFfuhs6rkiyTA==</a> (P-14)</li> <li><a href="https://www2.chemistry.msu.edu/faculty/reusch/virttxtjml/photchem.htm">https://www2.chemistry.msu.edu/faculty/reusch/virttxtjml/photchem.htm</a> (Photochemistry)</li> <li><a href="https://www2.chemistry.msu.edu/faculty/reusch/virttxtjml/pericycl.htm#top1">https://www2.chemistry.msu.edu/faculty/reusch/virttxtjml/pericycl.htm#top1</a> (Pericyclic reactions)</li> <li><a href="https://www2.chemistry.msu.edu/faculty/reusch/virttxtjml/synth1.htm#top2">https://www2.chemistry.msu.edu/faculty/reusch/virttxtjml/synth1.htm#top2</a> (Disconnection approach)</li> </ol> <p> </p> </div></div></div><div class="field field-name-field-academic-year field-type-taxonomy-term-reference field-label-above"><div class="field-label">Academic Year: </div><div class="field-items"><div class="field-item even"><a href="/academic-year/2025-2026" typeof="skos:Concept" property="rdfs:label skos:prefLabel" datatype="">2025-2026</a></div></div></div> Mon, 02 Jun 2025 05:21:04 +0000 ruchi.singh@iisuniv.ac.in 1948 at https://chemistry.iisuniv.ac.in Chemistry Laboratory VI https://chemistry.iisuniv.ac.in/courses/subjects/chemistry-laboratory-vi-4 <div class="field field-name-field-paper-code field-type-text field-label-inline clearfix"><div class="field-label">Paper Code: </div><div class="field-items"><div class="field-item even">25CCHY314</div></div></div><div class="field field-name-field-credits field-type-text field-label-inline clearfix"><div class="field-label">Credits: </div><div class="field-items"><div class="field-item even"> 02</div></div></div><div class="field field-name-field-periods field-type-number-decimal field-label-inline clearfix"><div class="field-label">Contact Hours: </div><div class="field-items"><div class="field-item even">60.00</div></div></div><div class="field field-name-field-maxmarks field-type-number-decimal field-label-inline clearfix"><div class="field-label">Max. Marks: </div><div class="field-items"><div class="field-item even">100.00</div></div></div><div class="field field-name-field-objective field-type-text-long field-label-above"><div class="field-label">Objective: </div><div class="field-items"><div class="field-item even"><p><strong>This course will enable the students to </strong></p> <p align="justify">detect the presence of oxygen containing functional groups and synthesize some important organic compounds by conventional and green methods.</p> <p align="justify"> </p> </div></div></div><div class="field field-name-field-course-outcomes field-type-text-with-summary field-label-above"><div class="field-label">Course Outcomes: </div><div class="field-items"><div class="field-item even"><table border="1" cellspacing="0" id="tab" style="width: 100%"> <thead> <tr> <th colspan="2" scope="col" style="width: 29%;"> <p align="justify" style="margin-left:36.0000pt;"><strong>Course</strong></p> </th> <th rowspan="2" scope="col" style="width: 32.36%;"> <p align="justify" style="margin-left:36.0000pt;"><strong>Learning Outcome</strong></p> <p align="justify" style="margin-left:36.0000pt;"><strong>(at course level)</strong></p> </th> <th rowspan="2" scope="col" style="width: 21.24%;"> <p style="margin-left:6.3000pt;"><strong>Learning and Teaching Strategies</strong></p> </th> <th rowspan="2" scope="col" style="width: 17.42%;"> <p style="margin-left:4.2000pt;"><strong>Assessment Strategies </strong></p> </th> </tr> </thead> <tbody> <tr> <td style="width:12.66%;"> <p align="center"><strong>Course Code</strong></p> </td> <td style="width:16.34%;"> <p align="center"><strong>Course</strong></p> <p align="center"><strong>Title</strong></p> </td> </tr> <tr> <td style="width:12.66%;"> <p style="margin-left:8.1000pt;"> </p> <p align="center"><strong>25CCHY314</strong></p> <p align="center" style="margin-left:8.1000pt;"> </p> </td> <td style="width:16.34%;"> <p align="center"> </p> <p align="center"><strong>Chemistry Laboratory </strong><strong>IV</strong></p> <p align="center"><strong>(</strong><strong>Practical</strong><strong>)</strong></p> <p align="center"> </p> </td> <td style="width:32.36%;"> <p align="justify"><strong>CO58:</strong> Identify the functional groups in simple organic compounds by performing step-wise qualitative tests and prepare suitable derivatives.</p> <p align="justify"><strong>CO59:</strong> Synthesize some important organic compounds through conventional methods as well as green methods and check their melting points and purity after recrystallization.</p> <p align="justify"><strong>CO</strong><strong>60</strong><strong>:</strong> Compile and report the results efficiently, and develop communications skills.</p> <p align="justify"><strong>CO</strong><strong>61</strong>: Contribute effectively in course-specific interaction.</p> </td> <td style="width:136px;"> <p><strong>Approach in teaching:</strong></p> <p>Power point presentation, laboratory instructions and demonstrations.</p> <p style="margin-left:36.0000pt;"> </p> <p style="margin-left:36.0000pt;"> </p> <p><strong>Learning activities for the students:</strong></p> <p>Peer learning, hands-on-learning, interpretation of data, record</p> <p>writing and learning through virtual labs.</p> <p> </p> </td> <td style="width:111px;"> <p align="justify">Conduction of experiments, lab records, viva voce.</p> <p> </p> <p> </p> </td> </tr> </tbody> </table> <p> </p> </div></div></div><div class="field field-name-field-unit1title field-type-text field-label-above"><div class="field-label">Unit I: </div><div class="field-items"><div class="field-item even"> </div></div></div><div class="field field-name-field-unit1description field-type-text-long field-label-hidden"><div class="field-items"><div class="field-item even"><p align="justify"><strong>Functional group tests</strong></p> <p align="justify">Determination of functional groups for alcohols, phenols, carbonyl and carboxylic acid group and preparation of their suitable derivatives</p> <p align="justify"> </p> <p align="justify"><strong>Organic preparations </strong>(Any six)</p> <p style="margin-left:18.2000pt;">· Benzolyation of one of the following amines (aniline, o-, m-, p- toluidines and o-, m-, p-anisidine) and one of the following phenols (β-naphthol, resorcinol, p-cresol) by Schotten-Baumann reaction.</p> <p style="margin-left:18.2000pt;">· Oxidation of ethanol/ isopropanol (Iodoform reaction).</p> <p style="margin-left:18.2000pt;">· Salicylic acid by green approach (using ceric ammonium nitrate).</p> <p style="margin-left:18.2000pt;">· Selective reduction of meta dinitrobenzene to m-nitroaniline.</p> <p style="margin-left:18.2000pt;">· Reduction of p-nitrobenzaldehyde by sodium borohydride.</p> <p style="margin-left:18.2000pt;">· Hydrolysis of amides and esters.</p> <p style="margin-left:18.2000pt;">· Semicarbazone of any one of the following compounds: acetone, ethyl methylketone, cyclohexanone, benzaldehyde.</p> <p style="margin-left:18.2000pt;">· Aldol condensation using either conventional or green method.</p> <p style="margin-left:18.2000pt;">· Benzil-Benzilic acid rearrangement.</p> <p style="margin-left:18.2000pt;">· The above derivatives should be prepared using 0.5-1g of the organic compound. The solid samples must be collected and may be used for recrystallization, melting point and TLC.</p> </div></div></div><div class="field field-name-field-essential-reading field-type-text-long field-label-above"><div class="field-label">Essential Readings: </div><div class="field-items"><div class="field-item even"><p style="margin-left:21.2500pt;">1. Practical Organic Chemistry; Fourth Edition; F.C. Mann, B.C. Saunders; Pearson Education Ltd., New Delhi, 2013.</p> <p style="margin-left:21.2500pt;">2. Vogel’s Textbook of Practical Organic Chemistry; Fifth Edition; B.S. Furniss, A.J. Hannaford, P.W.G. Smith, A.R. Tatchell ; Adission – Wesley Longman Ltd. England, 2015.</p> </div></div></div><div class="field field-name-field-references field-type-text-long field-label-above"><div class="field-label">References: </div><div class="field-items"><div class="field-item even"><p style="margin-left:21.2500pt;">1. Comprehensive Practical Organic Chemistry,Ahluwalia, V.K. & Aggarwal, R.,University Press (2000).</p> <p style="margin-left:21.2500pt;">2. Comprehensive Practical Organic Chemistry: Qualitative Analysis; Ahluwalia, V.K. & Dhingra, S. University Press (2000).</p> <p style="margin-left:21.2500pt;">3. Advanced University Practical Chemistry, Part I, First Edition; P.C. Kamboj, Vishal Publishing House, New Delhi; 2013.</p> <p align="justify" style="margin-left:22.5000pt;"> </p> <p style="margin-left:4.0500pt;"> </p> <p><strong>e-Resources:</strong></p> <p> </p> <p style="margin-left:21.2500pt;">1. <a href="https://www.youtube.com/watch?v=oROSQnzSdZE">https://www.youtube.com/watch?v=oROSQnzSdZE</a>(Preparation of Organic Compounds)</p> <p style="margin-left:21.2500pt;">2. <a href="https://www.tandfonline.com/doi/full/10.1080/17518253.2012.740078?cookieSet=1">https://www.tandfonline.com/doi/full/10.1080/17518253.2012.740078?cookieSet=1</a>(Green methodologies in organic synthesis)</p> <p style="margin-left:22.5000pt;"> </p> <p align="center"> </p> <p align="center"><strong>Scheme of Examination</strong></p> <p align="justify"> </p> <p align="justify">The duration of examination will be 5 hrs.</p> <p align="justify">The following exercises will be set in the examination</p> <p align="justify"> </p> <p align="justify">Organic Synthesis (one step) 30 marks</p> <p align="justify">Determination of Functional Group 25 marks</p> <p align="justify">Viva 15 marks</p> <p align="justify"><strong>Total</strong> <strong>70 marks</strong></p> <p align="justify"> </p> <p align="justify"><strong>Organic Synthesis </strong></p> <p align="justify">This exercise carries 30 marks. 4 marks out of 30 are reserved for neat, methodical and systematic working. The exercise amongst the candidates will be allotted by lot.</p> <p align="justify">The yield, purity, crystallization, recording of M.P. and proper presentation of the compound shall be taken into account while awarding marks.</p> <p align="justify"> </p> <p align="justify"><strong>Functional Group Determination</strong></p> <p align="justify">This exercise carries 25 marks. Two compounds (one solid and one liquid) will be provided to detect the functional group. Detection of each compound carries 10 marks. Preparation of one derivative carries 5 marks. The distribution of 10 marks will be as follows:</p> <p align="justify">Physical properties: colour, state, odour 1 mark</p> <p align="justify">Ignition test (Aliphatic/Aromatic) 1 mark</p> <p align="justify">Solubility 1 mark</p> <p align="justify">Action on litmus paper 1 mark</p> <p align="justify">Detection of functional group: Preliminary test 2 marks</p> <p align="justify">Confirmatory test of functional groups 2 marks</p> <p align="justify">M.P./B.P. 1 mark</p> <p align="justify">Result 1 mark</p> <p align="justify"> </p> <p align="justify"><strong>Viva</strong></p> <p align="justify">Oral questions shall generally be asked over the work assigned to the candidate. The purpose is to find out as to what extent the candidate has understood the basic principles.</p> <p> </p> </div></div></div><div class="field field-name-field-academic-year field-type-taxonomy-term-reference field-label-above"><div class="field-label">Academic Year: </div><div class="field-items"><div class="field-item even"><a href="/academic-year/2025-2026" typeof="skos:Concept" property="rdfs:label skos:prefLabel" datatype="">2025-2026</a></div></div></div> Sat, 31 May 2025 09:05:26 +0000 trapti.gupta@iisuniv.ac.in 1937 at https://chemistry.iisuniv.ac.in

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