Laboratory Course

Paper Code: 
CHY - 504
Credits: 
2
Contact Hours: 
60.00
Max. Marks: 
100.00
Unit I: 

Organic Chemistry 

Qualitative Analysis

Separation and identification of solid binary mixture using water/NaHCO3 /NaOH and preparation of suitable derivatives.

20.00 HRS

Physical / Analytical  Chemistry     (Any three)

Colorimetry

a) Record an absorption spectrum of a substance (KMnO4/K2Cr2O7) using a spectrophotometer and determine absorption maxima (λmax).

b) To verify the Beer-Lambert law for a compound( Potassium permanganate, copper sulphate, methylene blue etc. ) and determine the concentration of the substance using calibration curve.

c) Detection of adulteration of food stuffs - To detect the total dye content in sunset yellow colour

d) Water analysis- analysis of phosphorus in water.

Colorimetry

  1. Job’s method of continuous variation by iron-phenanthroline complex.
  2. Mole Ratio method by iron-phenanthroline complex.

Polarimeter

   c) To determine the specific rotation /unknown concentration of an    optically active compound (glucose/sucrose)

 Adsorption (Practice Exercise)

d) To study the adsorption of a solute (Acetic acid) on a dispersed solid (activated charcoal).

 

 

References: 
  1. Vogel’s Textbook of Practical Organic Chemistry; Fifth Edition; B.S. Furniss, A.J. Hannaford, P.W.D. Smith, A.R. Tatchell; Addison-Wesley Longman Ltd., England, 1998.
  2. Advanced Practical Physical Chemistry; Twenty-second Edition; J.B.Yadav; Goel Publishing House, Merrut, 2005.
  3. Advanced Practical Organic Chemistry, JagMohan , Himalaya Publishing House ,1992.

 

 

Academic Year: