Laboratory Course

Paper Code: 
CHY- 304
Credits: 
2
Contact Hours: 
60.00
Unit I: 

Inorganic Chemistry

 

Synthesis                                                                                                          10 hrs

a)      Preparation of Prussian blue Fe4[Fe(CN)6]3

b)      Preparation of Sodiumtrioxalatoferrate (III)

c)      Preparation of cis and trans-bisoxalatodiaquachromate (III).

d)      Preparation of Bis-Dimethylglyoxime-nickel (II)

 

Organic Chemistry                                                                     32 hrs

 

Qualitative Analysis

Identification of an organic compound through the functional group analysis, determination of melting point/boiling point and preparation of suitable derivatives.

Physical Chemistry                                                                      18 hrs

Thermochemistry

1.      To determine the enthalpy of neutralisation of strong acid and strong base.

2.      To determine the enthalpy of neutralization a weak acid/weak base versus strong base/strong acid and determine the enthalpy of ionization of weak acid/weak base.

 

Conductometry

To determine the strength of unknown acid (HCl/CH3COOH) conductometrically using standard alkali solution.

References: 
  1. Vogel’s Textbook of Practical Organic Chemistry; Fifth Edition; B.S. Furniss, A.J. Hannaford, P.W.D. Smith, A.R. Tatchell; Addison-Wesley Longman Ltd., England, 1998.
  2. Advanced Practical Physical Chemistry; Twenty-second Edition; J.B.Yadav; Goel Publishing House, Merrut,2005.
  3. Advanced Practical Inorganic Chemistry, Gurdeep Raj ,Goel Publishing House ,Meerut 2010.
  4. Advanced Practical Organic Chemistry , JagMohan , Himalaya Publishing House ,1992
Academic Year: 
2014-2015
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