Organic Chemistry 36 hrs
a) Aromatic Electrophilic Substitution
i) Acetylation – Acetylation of aniline/salicylic acid.
ii) Nitration - Preparation of 4-nitrosalicylic acid
ii) Bromination - Preparation of p-bromoacetanilide
b) Halogen Addition to C=C bond
i) Bromination of Trans Stilbene
c) [4+2] cycloaddition Reaction
i) Diel’s Alder reaction between furan and maleic acid
d) Pechmann Condensation for Coumarin synthesis
i) Clay catalysed solid state synthesis of 7-hydroxy -4-methyl coumarin
e) Diazotization/coupling
i) Preparation of methyl orange
Spectroscopy: Interpretation of IR and NMR spectra of simple organic compounds (ethanol, 1-propanol, 2-propanol, methylethanoate, ethyl acetate,stilbene, ethyl acetate, propanone etc).
Quantitative Analysis 12 hrs
a) To determine the neutralization equivalent of the acid.
b) Estimation of glucose by Fehling’s solution/Benedict’s solution method.
c) Estimation of saponification value of oil.